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Open-File Report 2008–1269

Prepared in cooperation with the National Park Service

Protocol for Monitoring Metals in Ozark National Scenic Riverways, Missouri: Version 1.0

By Christopher J. Schmitt, William G. Brumbaugh, John M. Besser, Jo Ellen Hinck, David E. Bowles, Lloyd W. Morrison, and Michael H. Williams

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Abstract

The National Park Service is developing a monitoring plan for the Ozark National Scenic Riverways in southeastern Missouri. Because of concerns about the release of lead, zinc, and other metals from lead-zinc mining to streams, the monitoring plan will include mining-related metals. After considering a variety of alternatives, the plan will consist of measuring the concentrations of cadmium, cobalt, lead, nickel, and zinc in composite samples of crayfish (Orconectes luteus or alternate species) and Asian clam (Corbicula fluminea) collected periodically from selected sites. This document, which comprises a protocol narrative and supporting standard operating procedures, describes the methods to be employed prior to, during, and after collection of the organisms, along with procedures for their chemical analysis and quality assurance; statistical analysis, interpretation, and reporting of the data; and for modifying the protocol narrative and supporting standard operating procedures. A list of supplies and equipment, data forms, and sample labels are also included. An example based on data from a pilot study is presented.

Version 1.0

Posted September 2008

For additional information contact:
Christopher Schmitt
USGS Columbia Environmental Research Center
Phone: (573) 875-5399
FAX: (573) 876-1896
Public Website: http://www.cerc.usgs.gov/index.htm

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Suggested citation:

Schmitt, C.J., Brumbaugh, W.G., Besser, J.M., Hinck, J.E., Bowles, D.E., Morrison, L.W., and Williams, M.H., 2008, Protocol for monitoring metals in Ozark National Scenic Riverways, Missouri: Version 1.0: U.S. Geological Survey Open-File Report 2008–1269, 42 p.



Contents

Abstract

Introduction

Purpose and Scope

Sampling Design

Methods

Operational Requirements

Procedure for Revising the Protocol and Archiving Previous Versions of the Protocol

Standard Operating Procedure 1: Preparation for Sampling, Version 1.0 (July 28, 2008)

Standard Operating Procedure 2: Collecting, Processing, and Preparing Samples of Crayfish and Asian Clams, Version 1.0 (July 28, 2008)

Standard Operating Procedure 3: After the Field Collections, Version 1.0 (July 28, 2008)

Standard Operating Procedure 4: Data Management, Version 1.0 (July 28, 2008)

Standard Operating Procedure 5: Data Analysis, Version 1.0 (July 28, 2008)

Standard Operating Procedure 6: Reporting, Version 1.0 (July 28, 2008)

Standard Operating Procedure 7: After the Field Season, Version 1.0 (July 28, 2008)

Standard Operating Procedure 8: Revising the Protocol, Version 1.0 (July 28, 2008)

Acknowledgments

References Cited


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Last modified: Wednesday, 07-Dec-2016 21:25:10 EST