Stream-Sediment Samples Reanalyzed for Major, Rare Earth, and Trace Elements from Ten 1:250,000-Scale Quadrangles, south-central Alaska, 2007-08
Metadata also available as
Metadata:
- Identification_Information:
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- Citation:
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- Citation_Information:
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- Originator: Bailey, Elizabeth A.
- Originator: Shew, Nora B.
- Originator: Labay, Keith A.
- Originator: Schmidt, Jeanine M.
- Originator: O'Leary, Richard M.
- Originator: Detra, David E.
- Publication_Date: 2010
- Title:
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Stream-Sediment Samples Reanalyzed for Major, Rare Earth, and Trace Elements from Ten 1:250,000-Scale Quadrangles, south-central Alaska, 2007-08
- Geospatial_Data_Presentation_Form: tabular data
- Series_Information:
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- Series_Name: U.S. Geological Survey Open-File Report
- Issue_Identification: 2010-1147
- Publication_Information:
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- Publication_Place: Reston, VA
- Publisher: U.S. Geological Survey
- Online_Linkage: <http://pubs.usgs.gov/of/2010/1147/>
- Description:
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- Abstract:
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During the 1960s through the 1980s, the U.S. Geological Survey (USGS) conducted reconnaissance geochemical surveys of the drainage basins throughout most of the Anchorage, Bering Glacier, Big Delta, Gulkana, Healy, McCarthy, Mount Hayes, Nabesna, Talkeetna Mountains, and Valdez 1:250,000-scale quadrangles in Alaska as part of the Alaska Mineral Resource Assessment Program (AMRAP). These geochemical surveys provide data necessary to assess the potential for undiscovered mineral resources on public and other lands, and provide data that may be used to determine regional-scale element baselines. This report provides new data for 366 of the previously collected stream-sediment samples. These samples were selected for reanalysis because recently developed analytical methods can detect additional elements of interest and have lower detection limits than the methods used when these samples were originally analyzed. These samples were all analyzed for arsenic by hydride generation atomic absorption spectrometry (HGAAS), for gold, palladium, and platinum by inductively coupled plasma-mass spectrometry after lead button fire assay separation (FA/ICP-MS), and for a suite of 55 major, rare earth, and trace elements by inductively coupled plasma-atomic emission spectrometry and inductively coupled plasma-mass spectrometry (ICP-AES-MS) after sodium peroxide sinter at 450 degrees Celsius.
- Purpose:
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These data may be helpful to locate areas of potential interest for ore minerals, to provide data that may be used to determine regional-scale element baselines, and to provide data for USGS mineral resource assessment studies.
- Time_Period_of_Content:
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- Time_Period_Information:
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- Range_of_Dates/Times:
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- Beginning_Date: 2007
- Ending_Date: 2008
- Currentness_Reference: years in which samples were analyzed
- Status:
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- Progress: Complete
- Maintenance_and_Update_Frequency: None planned
- Spatial_Domain:
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- Bounding_Coordinates:
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- West_Bounding_Coordinate: -150.00000
- East_Bounding_Coordinate: -141.0000
- North_Bounding_Coordinate: 64.5000
- South_Bounding_Coordinate: 60.7000
- Keywords:
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- Theme:
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- Theme_Keyword_Thesaurus: ISO 19115 Topic Category
- Theme_Keyword: geoscientificInformation
- Theme_Keyword: environment
- Theme_Keyword: sediments
- Theme_Keyword: geochemistry
- Theme_Keyword: mineral resources
- Theme_Keyword: geochemical data
- Theme_Keyword: mineral exploration
- Theme_Keyword: exploration geochemistry
- Theme_Keyword: sediment chemistry
- Theme_Keyword: environmental geochemistry
- Theme_Keyword: mineral resource assessment
- Theme_Keyword: major elements
- Theme_Keyword: trace elements
- Theme_Keyword: rare earth elements
- Place:
-
- Place_Keyword_Thesaurus: ISO 19115 Topic Category
- Place_Keyword: location
- Place_Keyword: United States of America
- Place_Keyword: Alaska
- Place_Keyword: East-Central Alaska
- Place_Keyword: Anchorage
- Place_Keyword: Gulkana
- Place_Keyword: Healy
- Place_Keyword: McCarthy
- Place_Keyword: Mount Hayes
- Place_Keyword: Nabesna
- Place_Keyword: Talkeetna Mountains
- Place_Keyword: Valdez
- Place_Keyword: Bering Glacier
- Place_Keyword: Big Delta
- Access_Constraints: None
- Use_Constraints: None
- Point_of_Contact:
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- Contact_Information:
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- Contact_Person_Primary:
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- Contact_Person: Bailey, Elizabeth A.
- Contact_Organization: U.S. Geological Survey, Alaska Science Center
- Contact_Position: Research Chemist
- Contact_Address:
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- Address_Type: Mailing address
- Address: 4210 University Drive
- City: Anchorage
- State_or_Province: Alaska
- Postal_Code: 99508-4626
- Country: United States of America
- Contact_Voice_Telephone: 1-907-786-7442
- Contact_Facsimile_Telephone: 1-907-786-7401
- Contact_Electronic_Mail_Address: <eabailey@usgs.gov>
- Browse_Graphic:
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- Browse_Graphic_File_Name: <http://pubs.usgs.gov/of/2010/1147/fig1.pdf>
- Browse_Graphic_File_Description:
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Map showing location of 366 stream-sediment samples reanalyzed by the U.S. Geological Survey in the Anchorage, Bering Glacier, Big Delta, Gulkana, Healy, McCarthy, Mount Hayes, Nabesna, Talkeetna Mountains, and Valdez 1:250,000-scale quadrangles, Alaska
- Browse_Graphic_File_Type: PDF (Portable Document Format)
- Data_Set_Credit:
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Matthew Granitto: USGS, Denver, CO, USGS National Geochemical Database (NGDB) organization and maintenance
Steven M. Smith: USGS, Denver, CO, USGS NGDB project leader
David E. Detra: USGS Denver, CO, Analytical chemistry methods information, analytical data quality assurance and control, contract chemistry manager
Richard M. O'Leary: USGS Denver, CO, Analytical chemistry methods information, analytical data quality assurance and control, sample preparation oversight
Timothy Brabets: USGS Anchorage, AK, technical reviewer
Bruce M. Gamble: USGS Anchorage, AK, technical reviewer
Theresa Taylor: USGS Anchorage, AK, metadata reviewer
Evan Thoms: USGS Anchorage, AK, metadata reviewer
- Data_Quality_Information:
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- Attribute_Accuracy:
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- Attribute_Accuracy_Report:
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The analytical methods used to generate the data in this report were selected by the authors. The accuracy of the data varies with the analytical methodology and with the concentration of the element being analyzed. Please see USGS Open-File Report 02-0223 (<http://pubs.usgs.gov/of/2002/ofr-02-0223/>) and the USGS Mineral Resources Program Contract Laboratory Method Summaries web site (<http://minerals.cr.usgs.gov/projects/analytical_chem/references.html>) for specific details on the sample preparation and analytical methods used for this report.
- Logical_Consistency_Report:
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All of the location coordinate and analytical data fields have been formatted as numeric fields. Maximum and minimum values were calculated to insure that valid results were reported for each analytical value; that is all values are greater than zero (0) and not less than the element lower reporting limit for each analytical method. Latitude/Longitude coordinates were checked to insure they plotted in the correct 1:250,000-scale quadrangle.
- Completeness_Report:
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Samples to be reanalyzed were randomly selected from 10 x 10 km (6.2 x 6.2 mi) grid cells that we overlaid on the study area to ensure a relatively even sample distribution. When available, two samples were selected from each cell. Archived material sufficient for re-analysis was not available for all samples initially selected. When possible, new selections were made in an attempt to continue to have two samples from each cell.
The selected samples were reanalyzed to determine if the original analyses are adequate for regional-scale mineral resource assessment, if the original data are adequate to determine regional-scale baselines for elements of interest, and to incorporate additional analyses such as platinum and palladium and rare earth elements (REE). Original analyses, many of which are by semiquantitative methods, may be found in the Rock Analysis and Storage System (RASS) component of the National Geochemical Database (NGDB), but are not included in this dataset.
The geographic extent of this area includes the Anchorage, Bering Glacier, Big Delta, Gulkana, Healy, McCarthy, Mount Hayes, Nabesna, Talkeetna Mountains, and Valdez 1:250,000-scale quadrangles in Alaska. All of the 366 samples retrieved from the Building 810 archive at the Denver Federal Center for this report were reanalyzed for As by hydride generation atomic absorption spectrometry (HGAAS), and for a suite of 55 major, rare earth, and trace elements by inductively coupled plasma-atomic emission spectrometry and inductively coupled plasma-mass spectrometry (ICP-AES-MS). Most of these samples were also reanalyzed for Au, Pd, and Pt by inductively coupled plasma-mass spectrometry after fire assay separation (FA/ICP_MS) however 16 samples did not contain enough material (30 g.) to be analyzed. These are noted in the data table with "ins" in the fields (columns) for Au, Pd, and Pt.
All sample analyses were completed in 2007-2008 at a laboratory under contract to the USGS. Contract laboratory oversight, data entry into the USGS National Geochemical Database, and analytical data QA/QC are managed by David E. Detra, David L. Fey, and Richard M. O'Leary at the USGS in Denver, CO.
This report consists of 3 files.
The first PDF file (OFR2010-1147.pdf) contains introductory and explanatory text and a table with the upper and lower reporting limits for each element analyzed by the various analytical methods used for this data set.
The second file is a PDF (fig1.pdf) image showing the location of the 366 stream-sediment samples reanalyzed for this report.
The third file contains the sample identification, location, and analytical data for each sample reported in MSExcel spreadsheet (table2.xls).
Abreviations used in the downloadable data table (table2.xls):
HGAAS: hydride genration atomic absorption spectrometry
FA/ICP_MS: fire assay with inductively coupled plasma-mass spectrometry finish
ICPAES_MS55: inductively coupled plasma-atomic emission spectrometry or inductively coupled plasma-mass spectrometry
ppb: parts per billion
ppm: parts per million
%: percent
<: less than the indicated lower limit of detection for the element as determined by the analytical method used
ins: insufficient sample for analysis
- Positional_Accuracy:
-
- Horizontal_Positional_Accuracy:
-
- Horizontal_Positional_Accuracy_Report:
-
Horizontal positions are specified in geographic coordinates, that is, latitude and longitude. Latitude and longitude values are specified in decimal degrees. The original sample location data were recorded in a variety of formats (decimal degrees, degrees plus decimal minutes, degrees-minutes-seconds). Most of the coordinates were originally determined in the field using clear mylar graticules overlaid on a paper 1:63,360-scale topographic base maps in degrees, minutes, and seconds or in the office using a tablet digitizer. When submitters reported locations as degrees, minutes, and seconds of latitude and longitude the accuracy should be within a few seconds or about 200 feet.
The horizontal datum used is North American Datum of 1927
The ellipsoid used is Clarke 1866
- Lineage:
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- Process_Step:
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- Process_Description:
-
Three hundred sixty six stream-sediment samples that were previously collected collected in west-central Alaska by several USGS scientists were retrieved from the USGS sample storage archive in Building 810 at the Denver Federal Center and chemically analyzed. All samples were analyzed for As by hydride generation atomic absorption spectrometry (HGAAS), for Au, Pd, and Pt by inductively coupled plasma-mass spectrometry after fire assay separation (FA/ICP_MS), and for a suite of 55 major, rare earth, and trace elements by inductively coupled plasma-atomic emission spectrometry and inductively coupled plasma-mass spectrometry (ICP-AES-MS).
2. Location and analytical data were compiled in spreadsheet form (table2.xls). Columns (fields) containing numeric data such as latitude, longitude, and analytical data were formatted as numeric fields and saved.
- Process_Date: 20100205
- Spatial_Data_Organization_Information:
-
- Direct_Spatial_Reference_Method: Point
- Point_and_Vector_Object_Information:
-
- SDTS_Terms_Description:
-
- SDTS_Point_and_Vector_Object_Type: Entity point
- Spatial_Reference_Information:
-
- Horizontal_Coordinate_System_Definition:
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- Geographic:
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- Latitude_Resolution: 0.001 degrees
- Longitude_Resolution: 0.001 degrees
- Geographic_Coordinate_Units: Decimal degrees
- Geodetic_Model:
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- Horizontal_Datum_Name: North American Datum of 1927 (NAD27)
- Ellipsoid_Name: Clarke 1866
- Semi-major_Axis: 6378206.4
- Denominator_of_Flattening_Ratio: 294.98
- Entity_and_Attribute_Information:
-
- Detailed_Description:
-
- Entity_Type:
-
- Entity_Type_Label: table2.xls
- Entity_Type_Definition:
-
This table contains analytical data for 366 stream-sediment samples. The fields (columns) consist of sample identification, location, and analytical information for each sample.
- Entity_Type_Definition_Source: U.S. Geological Survey
- Attribute:
-
- Attribute_Label: Map No.
- Attribute_Definition:
-
Unique identification number assigned by the authors to make reading the location figure easier. These numbers correspond to the sample location labels shown on plate1.pdf.
- Attribute_Definition_Source: U.S. Geological Survey, Nora B. Shew, Anchorage, AK - coauthor
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1
- Range_Domain_Maximum: 366
- Attribute:
-
- Attribute_Label: New Lab No.
- Attribute_Definition:
-
Each sample submitted for analyses is assigned a unique ID number by the USGS that is integrated with the USGS laboratory information storage system (LIMS) prior to submitting to a laboratory.
- Attribute_Definition_Source: U.S. Geological Survey, Richard M. O'Leary, Denver, CO
- Attribute_Domain_Values:
-
- Unrepresentable_Domain:
-
Alphanumeric data without scientific significance. Each value is assigned by the USGS/LIMS at the time of submittal and is unique.
- Attribute:
-
- Attribute_Label: Field_No.
- Attribute_Definition: Field number assigned by the submitter.
- Attribute_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Unrepresentable_Domain:
-
Alphanumeric data without scientific significance. Each value assigned by the submitter is unique.
- Attribute:
-
- Attribute_Label: Previous Job No.
- Attribute_Definition:
-
Assigned by the USGS. Samples are submitted by the USGS to a laboratory in jobs (groups) of samples. Each group of samples submitted for analyses is assigned a unique job number.
- Attribute_Definition_Source: U.S. Geological Survey, Richard M. O'Leary, Denver, CO
- Attribute_Domain_Values:
-
- Unrepresentable_Domain:
-
Alphanumeric data without scientific significance. Each value assigned by the USGS prior to submitting to a laboratory is unique to the group of samples submitted together. These values were assigned when the samples were originally submitted for preparation and analyses. The scheme used for Job No. has varied with time; some values are numeric and some values are combinations of letters and numbers.
- Attribute:
-
- Attribute_Label: Latitude
- Attribute_Definition:
-
North latitude of sample site reported in decimal degrees. (NAD27, Clarke 1866)
- Attribute_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 60.734
- Range_Domain_Maximum: 64.249
- Attribute_Units_of_Measure: decimal degrees
- Attribute:
-
- Attribute_Label: Longitude
- Attribute_Definition:
-
West longitude of sample site reported in negative decimal degrees. (NAD27, Clarke 1866)
- Attribute_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: -149.988
- Range_Domain_Maximum: -141.025
- Attribute_Units_of_Measure: decimal degrees
- Attribute:
-
- Attribute_Label: 1:250,000-scale quadrangle
- Attribute_Definition:
-
Name of the 1:250,000-scale quadrangle in which the sample was collected.
- Attribute_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: Anchorage
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: Bering Glacier
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: Big Delta
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: Gulkana
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: Healy
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: McCarthy
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: Mount Hayes
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: Nabesna
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: Talkeetna Mountains
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: Valdez
- Attribute:
-
- Attribute_Label: HGAAS As_ppm
- Attribute_Definition:
-
Concentration of arsenic in stream-sediment samples; determined by
hydride generation atomic absorption spectrometry (HGAAS)
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#M9>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.6
- Range_Domain_Maximum: 849
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
The optimum concentration range without sample dilution for As in various solid phase sample media is 0.6 ppm to 20 ppm. Data will be deemed acceptable if recovery of As is plus or minus 20% at five times the limit of detection (LOD) and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 20%.
- Attribute:
-
- Attribute_Label: FA/ICP_MS Au_ppb
- Attribute_Definition:
-
Concentration of gold in stream-sediment samples; determined by fire
assay with inductively coupled plasma_mass spectrometry finish (FA/ICP-MS)
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m20>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <1
- Enumerated_Domain_Value_Definition: below the lower limit of detection (1 ppb)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: ins
- Enumerated_Domain_Value_Definition: insufficient sample material for analysis
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1
- Range_Domain_Maximum: 1,780
- Attribute_Units_of_Measure: ppb (parts per billion)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data will be deemed acceptable if recovery of gold is plus or minus 20 percent (%) at five times the limit of detection (LOD) and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 20%. Sample weight is 30 g. (grams)
- Attribute:
-
- Attribute_Label: FA/ICP_MS Pd_ppb
- Attribute_Definition:
-
Concentration of palladium in stream-sediment samples; determined by
fire assay with inductively coupled plasma_mass spectrometry finish (FA/ICP-MS)
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m20>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <1
- Enumerated_Domain_Value_Definition: below the lower limit of detection (1 ppb)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: ins
- Enumerated_Domain_Value_Definition: insufficient sample material for analysis
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1
- Range_Domain_Maximum: 17
- Attribute_Units_of_Measure: ppb (parts per billion)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data will be deemed acceptable if recovery of palladium is plus or minus 20 percent (%) at five times the limit of detection (LOD) and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 20%. Sample weight is 30 g. (grams)
- Attribute:
-
- Attribute_Label: FA/ICP_MS Pt_ppb
- Attribute_Definition:
-
Concentration of platinum in stream-sediment samples; determined by fire
assay with inductively coupled plasma_mass spectrometry finish (FA/ICP-MS)
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m20>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <0.5
- Enumerated_Domain_Value_Definition: below the lower limit of detection (0.5 ppb)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: ins
- Enumerated_Domain_Value_Definition: insufficient sample material for analysis
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.5
- Range_Domain_Maximum: 11.1
- Attribute_Units_of_Measure: ppb (parts per billion)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data will be deemed acceptable if recovery of platinum is plus or minus 20 percent (%) at five times the limit of detection (LOD) and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 20%. Sample weight is 30 g. (grams)
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Al_%
- Attribute_Definition:
-
Concentration of aluminum in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1.40
- Range_Domain_Maximum: 10.8
- Attribute_Units_of_Measure: % (percent)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for aluminum is ±15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Ca_%
- Attribute_Definition:
-
Concentration of calcium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, Survey, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.13
- Range_Domain_Maximum: 25.1
- Attribute_Units_of_Measure: % (percent)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for calcium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Fe_%
- Attribute_Definition:
-
Concentration of iron in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.94
- Range_Domain_Maximum: 12.4
- Attribute_Units_of_Measure: % (percent)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for iron is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 K_%
- Attribute_Definition:
-
Concentration of potassium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.04
- Range_Domain_Maximum: 3.49
- Attribute_Units_of_Measure: % (percent)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for potassium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Mg_%
- Attribute_Definition:
-
Concentration of magnesium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.08
- Range_Domain_Maximum: 6.31
- Attribute_Units_of_Measure: % (percent)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for magnesium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Mn_%
- Attribute_Definition:
-
Concentration of manganese in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.01
- Range_Domain_Maximum: 0.45
- Attribute_Units_of_Measure: % (percent)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for manganese is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 P_%
- Attribute_Definition:
-
Concentration of phosphorus in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.02
- Range_Domain_Maximum: 0.32
- Attribute_Units_of_Measure: % (percent)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for phosphorus is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Ti_%
- Attribute_Definition:
-
Concentration of titanium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.07
- Range_Domain_Maximum: 3.93
- Attribute_Units_of_Measure: % (percent)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for titanium is ±15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Ag_ppm
- Attribute_Definition:
-
Concentration of silver in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <1
- Enumerated_Domain_Value_Definition: below the lower limit of detection (1 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1
- Range_Domain_Maximum: 10
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for silver is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 As_ppm
- Attribute_Definition:
-
Concentration of arsenic in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <30
- Enumerated_Domain_Value_Definition: below the lower limit of detection (30 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: ins
- Enumerated_Domain_Value_Definition: insufficient sample material for analysis
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 30
- Range_Domain_Maximum: 850
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for arsenic is pus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Ba_ppm
- Attribute_Definition:
-
Concentration of barium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 33
- Range_Domain_Maximum: 4,480
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for barium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Be_ppm
- Attribute_Definition:
-
Concentration of beryllium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <5
- Enumerated_Domain_Value_Definition: below the lower limit of detection (5 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 5
- Range_Domain_Maximum: 13
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for berylium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Bi_ppm
- Attribute_Definition:
-
Concentration of bismuth in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <0.1
- Enumerated_Domain_Value_Definition: below the lower limit of detection (0.1 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.1
- Range_Domain_Maximum: 1.1
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for bismuth is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Cd_ppm
- Attribute_Definition:
-
Concentration of cadmium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <0.2
- Enumerated_Domain_Value_Definition: below the lower limit of detection (0.2 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.2
- Range_Domain_Maximum: 50.9
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for cadmium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Ce_ppm
- Attribute_Definition:
-
Concentration of cerium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 3.4
- Range_Domain_Maximum: 380
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for cerium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Co_ppm
- Attribute_Definition:
-
Concentration of cobalt in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.6
- Range_Domain_Maximum: 51.5
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for cobalt is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Cr_ppm
- Attribute_Definition:
-
Concentration of chromium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 10
- Range_Domain_Maximum: 3,070
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for chromium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Cs_ppm
- Attribute_Definition:
-
Concentration of cesium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.1
- Range_Domain_Maximum: 11.4
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for cesium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Cu_ppm
- Attribute_Definition:
-
Concentration of copper in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 5
- Range_Domain_Maximum: 216
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for copper is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Dy_ppm
- Attribute_Definition:
-
Concentration of dysprosium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1.29
- Range_Domain_Maximum: 15.8
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for dysprosium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Er_ppm
- Attribute_Definition:
-
Concentration of erbium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.81
- Range_Domain_Maximum: 10.5
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for erbium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Eu_ppm
- Attribute_Definition:
-
Concentration of europium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.36
- Range_Domain_Maximum: 2.46
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for europium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Ga_ppm
- Attribute_Definition:
-
Concentration of gallium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 4
- Range_Domain_Maximum: 26
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for galium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Gd_ppm
- Attribute_Definition:
-
Concentration of gadollinium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1.00
- Range_Domain_Maximum: 20.4
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for gadolinium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Ge_ppm
- Attribute_Definition:
-
Concentration of germanium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <0.2
- Enumerated_Domain_Value_Definition: below the lower limit of detection (0.2 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1
- Range_Domain_Maximum: 3
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for germanium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Hf_ppm
- Attribute_Definition:
-
Concentration of hafnium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <1
- Enumerated_Domain_Value_Definition: below the lower limit of detection (1 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1
- Range_Domain_Maximum: 46
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for hafnium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Ho_ppm
- Attribute_Definition:
-
Concentration of holmium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.26
- Range_Domain_Maximum: 3.20
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for holmium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 In_ppm
- Attribute_Definition:
-
Concentration of indium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <0.2
- Enumerated_Domain_Value_Definition: below the lower limit of detection (0.2 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.3
- Range_Domain_Maximum: 0.3
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for indium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 La_ppm
- Attribute_Definition:
-
Concentration of lanthanum in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1.4
- Range_Domain_Maximum: 186
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for lanthanum is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Li_ppm
- Attribute_Definition:
-
Concentration of lithium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <10
- Enumerated_Domain_Value_Definition: below the lower limit of detection (10 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 10
- Range_Domain_Maximum: 80
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for lithium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Lu_ppm
- Attribute_Definition:
-
Concentration of lutetium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.10
- Range_Domain_Maximum: 1.37
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for lutetium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Mo_ppm
- Attribute_Definition:
-
Concentration of molybdenum in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <2
- Enumerated_Domain_Value_Definition: below the lower limit of detection (2 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 2
- Range_Domain_Maximum: 15
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for molybdenum is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Nb_ppm
- Attribute_Definition:
-
Concentration of niobium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1
- Range_Domain_Maximum: 58
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for nioboim is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Nd_ppm
- Attribute_Definition:
-
Concentration of neodymium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 2.5
- Range_Domain_Maximum: 161
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for neodymium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Ni_ppm
- Attribute_Definition:
-
Concentration of nickel in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <5
- Enumerated_Domain_Value_Definition: below the lower limit of detection (5 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 5
- Range_Domain_Maximum: 421
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for nickel is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Pb_ppm
- Attribute_Definition:
-
Concentration of lead in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <5
- Enumerated_Domain_Value_Definition: below the lower limit of detection (5 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 5
- Range_Domain_Maximum: 520
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for lead is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Pr_ppm
- Attribute_Definition:
-
Concentration of praeseodymium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.48
- Range_Domain_Maximum: 42.4
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for praeseodymium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Rb_ppm
- Attribute_Definition:
-
Concentration of rubidium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.7
- Range_Domain_Maximum: 170
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for rubidium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Sb_ppm
- Attribute_Definition:
-
Concentration of anitmony in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <0.1
- Enumerated_Domain_Value_Definition: below the lower limit of detection (0.1 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.1
- Range_Domain_Maximum: 21.2
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for antimony is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Sc_ppm
- Attribute_Definition:
-
Concentration of scandium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <5
- Enumerated_Domain_Value_Definition: below the lower limit of detection (5 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 5
- Range_Domain_Maximum: 47
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for scandium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Sm_ppm
- Attribute_Definition:
-
Concentration of samarium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.8
- Range_Domain_Maximum: 29.6
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for samarium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Sn_ppm
- Attribute_Definition:
-
Concentration of tin in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <1
- Enumerated_Domain_Value_Definition: below the lower limit of detection (1 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1
- Range_Domain_Maximum: 76
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for tin is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Sr_ppm
- Attribute_Definition:
-
Concentration of strontium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 38
- Range_Domain_Maximum: 923
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for strontium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Ta_ppm
- Attribute_Definition:
-
Concentration of tantalum in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <0.5
- Enumerated_Domain_Value_Definition: below the lower limit of detection (0.5 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.5
- Range_Domain_Maximum: 3.5
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for tantalum is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Tb_ppm
- Attribute_Definition:
-
Concentration of terbium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.18
- Range_Domain_Maximum: 3.18
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for terbium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Th_ppm
- Attribute_Definition:
-
Concentration of thorium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.3
- Range_Domain_Maximum: 160
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for thorium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Tl_ppm
- Attribute_Definition:
-
Concentration of thallium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <0.5
- Enumerated_Domain_Value_Definition: below the lower limit of detection (0.5 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.5
- Range_Domain_Maximum: 2.8
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for thallium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Tm_ppm
- Attribute_Definition:
-
Concentration of thulium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.11
- Range_Domain_Maximum: 1.55
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for thulium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 U_ppm
- Attribute_Definition:
-
Concentration of uranium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.08
- Range_Domain_Maximum: 47.7
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for uranium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 V_ppm
- Attribute_Definition:
-
Concentration of vanadium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 24
- Range_Domain_Maximum: 455
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for vanadium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 W_ppm
- Attribute_Definition:
-
Concentration of tungsten in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Enumerated_Domain:
-
- Enumerated_Domain_Value: <1
- Enumerated_Domain_Value_Definition: below the lower limit of detection (1 ppm)
- Enumerated_Domain_Value_Definition_Source: U.S. Geological Survey
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 1
- Range_Domain_Maximum: 102
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for tungsten is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Y_ppm
- Attribute_Definition:
-
Concentration of yttrium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 6.8
- Range_Domain_Maximum: 89.7
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for yttrium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Yb_ppm
- Attribute_Definition:
-
Concentration of ytterbium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
-
- Range_Domain:
-
- Range_Domain_Minimum: 0.7
- Range_Domain_Maximum: 9.9
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for ytterbium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Zn_ppm
- Attribute_Definition:
-
Concentration of zinc in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
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- Range_Domain_Maximum: 2,100
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for zinc is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Attribute:
-
- Attribute_Label: ICPAES_MS55 Zr_ppm
- Attribute_Definition:
-
Concentration of zirconium in stream-sediment samples; determined by
inductively coupled plasma atomic emission spectrometry or mass
spectrometry (ICP-AES-MS) following sodium peroxide sinter at 450 degrees Celsius
- Attribute_Definition_Source:
-
U.S. Geological Survey, Central Mineral and Environmental Resources Science Center (CMERSC) Analytical Chemistry, David E. Detra, Denver, CO and <http://minerals.cr.usgs.gov/projects/analytical_chem/references.html#m22>
- Attribute_Domain_Values:
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- Range_Domain_Maximum: 1,810
- Attribute_Units_of_Measure: ppm (parts per million)
- Attribute_Value_Accuracy_Information:
-
- Attribute_Value_Accuracy_Explanation:
-
Data is deemed acceptable if recovery for zirconium is plus or minus 15% at five times the lower limit of detection (LOD) for each element and the calculated percent relative standard deviation (RSD) of duplicate samples is no greater than 15%.
- Distribution_Information:
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- Distributor:
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- Contact_Information:
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- Contact_Organization_Primary:
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- Contact_Organization: USGS Information Services
- Contact_Address:
-
- Address_Type: Mailing address
- Address: Box 25286, Denver Federal Center
- City: Denver
- State_or_Province: CO
- Postal_Code: 80225-0046
- Country: United States
- Contact_Voice_Telephone: 1-888-ASK-USGS (1-888-275-8747) (voice)
- Contact_Facsimile_Telephone: 1-303-202-4695 (FAX)
- Contact_Electronic_Mail_Address: infoservices@usgs.gov
- Resource_Description: USGS Open-File Report 2010-1147
- Distribution_Liability:
-
The USGS makes no guarantee or warranty concerning the accuracy of information contained in the geographic data. The USGS further makes no warranties, either expressed or implied as to any other matter whatsoever, including, without limitation, the condition of the product, or its fitness for any particular purpose. The burden for determining fitness for use lies entirely with the user. Although this data has been processed successfully on computers at the USGS, no warranty, expressed or implied, is made by the USGS regarding the use of this data on any other system, nor does the fact of distribution constitute or imply any such warranty. In no event shall the USGS have any liability whatsoever for payment of any consequential, incidental, indirect, special, or tort damages of any kind, including, but not limited to, any loss of profits arising out of use of or reliance on the geographic data or arising out of the delivery, installation, operation, or support by the USGS
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- Digital_Form:
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- Digital_Transfer_Information:
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- Format_Name: XLS
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tabular data with sample identification, location information, and chemical analyses of stream-sediment samples
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- Format_Name: PDF
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- Digital_Form:
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- Format_Name: html, xml, txt
- Format_Information_Content:
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metadata files in FAQ-style HTML, standard HTML, XML, and TXT formats
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- Network_Resource_Name: <http://pubs.usgs.gov/of/20101147/2010-1147.zip>
- Fees: none
- Turnaround: Digital downloads: less than 30 minutes for most files
- Metadata_Reference_Information:
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- Metadata_Date: 20100625
- Metadata_Review_Date: 20100205
- Metadata_Contact:
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- Contact_Information:
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- Contact_Person_Primary:
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- Contact_Person: Bailey, Elizabeth A.
- Contact_Organization: U.S. Geological Survey, Alaska Science Center
- Contact_Position: Research Chemist
- Contact_Address:
-
- Address_Type: Mailing address
- Address: 4210 University Drive
- City: Anchorage
- State_or_Province: Alaska
- Postal_Code: 99508-4626
- Country: United States
- Contact_Voice_Telephone: 1-907-786-7442
- Contact_Facsimile_Telephone: 1-907-786-7401
- Contact_Electronic_Mail_Address: eabailey@usgs.gov
- Metadata_Standard_Name: Content Standard for Digital Geospatial Metadata
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Generated by mp version 2.9.8 on Thu Aug 19 13:19:46 2010