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The Chemical Analysis of Argonne Premium Coal Samples

Edited by Curtis A. Palmer
U.S. Geological Survey Bulletin 2144


Determination of 29 Elements in 8 Argonne Premium Coal Samples by Instrumental Neutron Activation Analysis

By Curtis A. Palmer

Table 2. Concentrations (in micrograms per gram, µg/g) of 29 elements in Argonne Premium Coal samples -- continued.

[Concentrations weredetermined by instrumental neutron activation analysis (INAA). Errors in percent are based on one-sigma counting statistics only.

Element PITT PC-4-1 PITT PC-4-2 PITT PC-4-3 POC PC-5-1 POC PC-5-2 POC PC-5-3 UT PC-6-1 UT PC-6-2 UT PC-6-3
Na 343±2% 343±3% 344±3% 797±2% 773±2% 778±2% 1,485±2% 1,472±2% 1,425±2%
K 1,090±5% 1,120±6% 1,090±7% 284±11% 260±14% 330±15% 180±25% <250 252±12%
Sc 2.61±2% 2.56±1% 2.55±1% 1.80±2% 1.79±2% 1.77±1% .832±2% .801±1% .805±2%
Cr 15.0±3% 15.0±3% 14.5±3% 9.3±4% 9.06±3% 8.85±3% 5.25±4% 5.03±4% 5.62±3%
Fe 13,600±2% 13,400±2% 13,300±2% 5,040±2% 5,210±2% 5,020±2% 3,270±2% 3,100±2% 3,150±2%
Co 2.65±3% 2.61±4% 2.60±6% 4.09±2% 4.13±2% 3.98±2% 1.01±2% .992±3% 1.00±2%
Ni 9.4±21% 11.3±17% <12 9.2±17% 8.5±19% 8.2±19% <3 3.6±32% 3.7±26%
Zn 8.9±4% 7.8±7% 10.5±12% 5.74±5% 6.15±5% 7.3±5% 4.80±5% 7.43±4% 6.82±4%
As 8.44±3% 8.30±3% 8.5±4% 10.43±3% 10.6±3% 9.89±3% .51±7% .50±9% .44±8%
Se 1.49±7% 1.60±7% 1.34±7% 2.3±28% 2.5±18% 2.601±11% 1.03±10% 1.16±10% 1.03±8%
Br 15.7±8% 15.5±8% 15.5±8% 50±8% 50±8% 49±8% 1.14±5 1.06±5% 1.05±5%
Rb 9.0±16% 7.2±16% 7.1±16% <6 <6 <3 <2 1.00±22% .95±25%
Sr 58±12% 61±22% 65±19% 97±23% 116±7% 101±11% 71±7% 68±8% 70±8%
Sb .239±6% .240±5% .221±6% .625±4% .458±4% .535±4% 118±7% .098±9% .106±8%
Cs .737±4% .69±9% .67±8% .256±5% .283±17% .247±11% .123±6% .148±6% .119±11%
Ba 44±13% 51±11% 44±12% 197±5% 203±5% 193±4% 35.7±8% 38.1±8% 47±7%
La 6.19±3% 6.15±3% 6.11±3% 6.78±3% 6.77±3% 6.73±3% 3.41±3% 3.27±3% 3.24±3%
Ce 11.5±3% 11.5±5% 11.1±3% 11.6±3% 11.8±3% 11.5±3% 4.88±3% 4.67±3% 4.84±3%
Nd <12 <8 <10 <18 <16 <14 <3 2.5±6% 1.6±26
Sm 1.100±2% 1.09±2% 1.09±2% 1.23±2% 1.21±2% 1.21±2% .517±3% .500±3% .507±3%
Eu .221±4% .214±4% .208±6% .243±4% .241±4% .218±10% .100±6% .098±5% .098±4%
Tb .133±5% .131±10% .132±8% .158±6% .173±4% .169±4% .065±5% .054±5% .054±5%
Yb .478±5% .463±5% .468±5% .555±5% .56±10% .545±5% .204±7% .198±15% .211±18%
Lu .121±6% .117±10% .120±5% .132±5% .142±5% .132±5% .036±9% .026±11% .029±7%
Hf .518±4% .49±8% .500±4% .441±6% .429±4% .444±4% .478±3% .499±5% .458±3%
Ta .168±5% .163±5% .165±5% .117±12% .108±8% .123±6% .060±7% .065±7% .061±6%
W .79±6% .80±8% .76±8% .84±7% .91±8% .77±8% .42±10% .40±11% .38±9%
Th 1.53±3% 1.46±3% 1.44±3% 1.19±3% 1.12±8% 1.17±3% .609±3% .614±3% .622±3%
U .36±13% .37±10% .45±11% .47±16% .51±13% .55±13% .76±8% .70±8% .76±9%
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