The Chemical Analysis of Argonne Premium Coal Samples
Edited by Curtis A. Palmer
1997
U.S. Geological Survey Bulletin 2144
Determination of 62 Elements in 8 Argonne Premium Coal Ash Samples by Automated Semiquantitative Direct-Current Arc Atomic Emission Spectrography
By Carol J. Skeen, B.J. Libby, and W.B. Crandell
Table 3. Element concentrations determined by direct-current arc spectrographic analyses of the Argonne Premium Coal samples -- continued.
Element | UT PC-6-1 | UT PC-6-2 | UT PC-6-3 | WV PC-7-1 | WV PC-7-2 | WV PC-7-3 | ND PC-8-1 | ND PC-8-2 | ND PC-8-3 |
Si (%) | 16 | 20 | 20 | 22 | 30 | 28 | 5.7 | 6.6 | 6.6 |
Al | 6.8 | 7.8 | 6.3 | 17 | 22 | 21 | 2.2 | 3.0 | 2.2 |
Fe | 4.6 | 5.9 | 5.1 | 1.8 | 2.3 | 2.1 | 3.7 | 4.5 | 3.5 |
Mg | .93 | .82 | .89 | .66 | .43 | .40 | 5.5 | 5.4 | 5.3 |
Ca | 6.0 | 6.3 | 6.3 | .40 | .31 | .49 | 13 | 14 | 15 |
Na | 1.9 | 1.4 | 1.4 | .19 | .18 | .19 | H | 2.6 | H |
K | .47 | .31 | .36 | 2.0 | 1.7 | 1.8 | .40 | .35 | .41 |
Ti | .40 | .43 | .40 | .95 | .91 | .90 | .18 | .18 | .20 |
P | <.068 | <.068 | <.068 | .086 | <.068 | <.068 | <.13 | .11 | .098 |
Mn | .014 | .010 | .016 | .0092 | .012 | .010 | .11 | .11 | .11 |
Ag (µg/g) | 12 | 8.9 | 9.6 | 2.6 | 2.2 | 2.2 | <.10 | <.10 | <.10 |
As | <220 | <220 | <220 | <220 | <220 | <220 | <220 | <220 | <220 |
Au | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 |
B | >1,000 | >1,000 | >1,000 | 150 | 480 | 250 | 500 | 800 | 810 |
Ba | 750 | 670 | 900 | 660 | 740 | 640 | 5,300 | 7,400 | 5,700 |
Be | 3.3 | 5.2 | 4.4 | 15 | 16 | 16 | 2.8 | 3.5 | 2.4 |
Bi | <22 | <22 | <22 | <22 | <22 | <22 | <22 | <22 | <22 |
Cd | <22 | <22 | <22 | <22 | <22 | <22 | <22 | <22 | <22 |
Ce | 160 | 160 | 130 | 130 | 140 | 130 | <63 | <63 | <63 |
Co | 15 | 13 | 14 | 3630 | 31 | 5.7 | 6.0 | 5.7 | 5.7 |
Cr | 110 | 85 | 120 | 220 | 180 | 210 | 25 | 25 | 26 |
Cu | 69 | 52 | 66 | 90 | 85 | 68 | 41 | 40 | 75 |
Dy | <10 | <10 | <10 | <10 | <10 | <10 | <10 | <10 | <10 |
Er | <4.6 | <4.6 | <4.6 | <4.6 | <4.6 | <4.6 | <4.6 | <4.6 | <4.6 |
Eu | <.68 | <.68 | 2.5 | 2.4 | 2.5 | 4.6 | <.68 | <.68 | <.68 |
Ga | 32 | 19 | 28 | 68 | 56 | 59 | 19 | 16 | 20 |
Gd | <22 | <22 | <22 | <22 | <22 | <22 | <22 | <22 | <22 |
Ge | <4.6 | <4.6 | <4.6 | 5.5 | <4.6 | 6.2 | <4.6 | <4.6 | <4.6 |
Hf | <10 | <10 | <10 | <10 | <10 | <10 | <10 | <10 | <10 |
Ho | <1.5 | <1.5 | <1.5 | 3.2 | <1.5 | 1.7 | <1.5 | <1.5 | <1.5 |
In | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 |
Ir | <10 | <10 | <10 | <10 | <10 | <10 | <10 | <10 | <10 |
La | 66 | 64 | 62 | 72 | 74 | 64 | 37 | 40 | 39 |
Lu | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 | <6.8 |
Mo | 12 | 8.4 | 11 | 7.0 | 8.4 | 6.3 | 8.6 | 8.2 | 8.7 |
Nb | 10 | 11 | 12 | 13 | 19 | 23 | 6.6 | 5.3 | 6.4 |
Nd | 64 | <150 | <150 | 97 | 100 | 90 | <32 | <32 | <150 |
Ni | 84 | 89 | 87 | 120 | 100 | 110 | 17 | 17 | 22 |
Os | <10 | <10 | <10 | <10 | <10 | <10 | <10 | <10 | <10 |
Pb | 45 | 36 | 43 | 93 | 81 | 69 | 28 | 22 | 32 |
Pd | <.68 | <.68 | <.68 | <.68 | <.68 | <.68 | <.68 | <.68 | <.68 |
Pr | 9.5 | 9.3 | 8.4 | 10 | 9.3 | <6.8 | <6.8 | <6.8 | 7.3 |
Pt | <1.5 | <1.5 | <1.5 | <1.5 | <1.5 | <1.5 | <1.5 | <1.5 | <1.5 |
Re | <10 | <10 | <10 | <10 | <10 | <10 | <10 | <10 | <10 |
Rh | <1.5 | <1.5 | <1.5 | <1.5 | <1.5 | <1.5 | <1.5 | <1.5 | <1.5 |
Ru | <1.0 | <1.0 | <1.0 | <1.0 | <1.0 | <1.0 | <1.0 | <1.0 | <1.0 |
Sb | <32 | <32 | <32 | <32 | <32 | <32 | <32 | <32 | <32 |
Sc | 16 | 15 | 14 | 36 | 31 | 32 | 9.2 | 9.1 | 10 |
Sm | 8.0 | 8.2 | 7.8 | 8.9 | 8.7 | <3.2 | <3.2 | <3.2 | 4.9 |
Sn | 8.8 | 5.9 | 9.4 | 11 | 8.4 | 10 | <4.6 | <4.6 | 13 |
Sr | 1,800 | 2,000 | 2,000 | 390 | 320 | 370 | 6,200 | 6300 | 7300 |
Ta | <320 | <320 | <320 | <320 | <320 | <320 | <320 | <320 | <320 |
Tb | <32 | <32 | <32 | <32 | <32 | <32 | <32 | <32 | <32 |
Th | <46 | <46 | <46 | <46 | <46 | <46 | <46 | <46 | <46 |
Tl | <10 | <10 | <10 | <10 | <10 | <10 | <1015 | <10 | <10 |
Tm | <3.2 | <3.2 | <3.2 | <3.2 | <3.2 | <3.2 | <3.2 | <3.2 | <3.2 |
U | <150 | <150 | <150 | <150 | <150 | <150 | <150 | <150 | <150 |
V | 82 | 78 | 79 | 160 | 180 | 150 | 38 | 38 | 37 |
W | <10 | <10 | <10 | <10 | <10 | <10 | <10 | <10 | <10 |
Y | 41 | 42 | 34 | 50 | 52 | 39 | 24 | 27 | 25 |
Yb | 4.9 | 4.4 | 4.6 | 9.2 | 7.3 | 7.1 | 2.3 | 2.0 | 2.1 |
Zr | 260 | 280 | 200 | 200 | 150 | 140 | 130 | 130 | 140 |
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