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North Carolina
Subcontractors for the Savannah River Laboratory (SRL) collected at least 6,666 stream-sediment, 295 surface-water, and 5,778 ground-water samples within 100 counties from North Carolina as part of the NURE Hydrogeochemical and Stream Sediment Reconnaissance (HSSR) program. The sediment samples were collected during June - December 1976; July - August 1977; and April - May 1978, and water samples were collected during December 1976 - August 1977 and June - July 1978. Sample coverage included portions of the Beaufort, Charlotte, Chattanooga, Currituck Sound, Florence, Georgetown, Greensboro, Greenville, Johnson City, Knoxville, Manteo, Norfolk, Raleigh, Rocky Mount, Rome, Spartanburg, and Winston-Salem 1:250,000-scale quadrangles. (A total of 502 stream-sediment, 858 ground-water, and 28 stream-water samples were collected within the Rocky Mount quadrangle.) These samples were sent to SRL for analysis of uranium and additional elements (16 in sediments and 9 in waters). SRL was able to analyze 6,597 sediments and 6,040 waters from North Carolina; this includes all 502 sediment and 886 water samples from the Rocky Mount quadrangle. The analytical and site location data for all North Carolina samples were released in the North and South Carolina Data Report [GJBX-102(82)].

SRL sent 4,677 sediment samples from North Carolina to an unnamed contract laboratory for "Supplemental Analyses." Supplemental analytical determinations for up to 23 elements were reported for 4,660 of these samples in the North and South Carolina Data Report [GJBX-102(82)]. The digital data file accompanying this report include Supplemental Analyses for 105 North Carolina sediment samples within the Rocky Mount quadrangle.

SRL: Rocky Mount and Manteo Quadrangles
SRL released a separate quadrangle report for the Rocky Mount and Manteo NTMS quadrangle, which includes data for 501 stream-sediment, 859 ground-water, and 28 stream-water samples (500 stream-sediment, 857 ground-water, and 28 stream-water samples collected within the Rocky Mount quadrangle). With minor differences, these sample data are the same as the that for corresponding samples found in the North and South Carolina State reports. SRL released the analytical data as the Rocky Mount and Manteo Quadrangles GJBX-16(81) Preliminary Basic Data Report. The site coding information for this data set is summarized within the text of this report.

Gold Analyses
Data for gold analyses of sediments by SRL neutron activation were released in the GJBX-135(82) summary report. The introduction of that report states:

"This report contains previously unreported neutron-activation analyses of gold in sediment samples determined at SRL. These data were not included in the standard SRL NURE data reports because the gold spectrum was not measured in the original analytical procedure and the report format was designed without the gold analyses being included. Gold analyses became available as the analytical procedure was refined, but the report format was not modified to incorporate these data."

Only those sediment samples that had detectable concentrations of gold by neutron activation analysis were given in the GJBX-135(82) report. Sediment samples with concentrations below detection limits were not reported and can only be ascertained by identifying which samples were actually analyzed by neutron activation at SRL.

Summary Tables
Because of the various laboratories and analytical methods used, some SRL samples may have been analyzed once, twice, or not at all. The following table summarizes the analysis of Rocky Mount quadrangle samples.

The following is a list of all sample types collected and reported for NURE studies in the Rocky Mount quadrangle.

These Rocky Mount quadrangle samples were analyzed by one or more of the following methods:

Sediment Samples

• SR1: Savannah River Neutron Activation Analysis - Neutron Counting of sediments for U.
• SR2: Savannah River Neutron Activation Analysis of sediments for Al, Ce, Dy, Eu, Fe, Hf, La, Lu, Mn, Na, Sc, Sm, Th, Ti, V, and Yb. (Note: Au values were reported later for this method.)
• SR3-AA: Savannah River (Supplemental Analysis by contract Laboratory) Atomic Absorption Spectroscopy Analysis of sediments for Ag, Ba, Be, Co, Cr, Cu, Mg, Mo, Ni, Pb, Sn, Sr, Y, and Zn.
• SR3-CA: Savannah River (Supplemental Analysis by contract Laboratory) Colorimetric Analysis of sediments for Nb, P, and W.
• SR3-FE: Savannah River (Supplemental Analysis by contract Laboratory) Flame Emission Analysis of sediments for K and Li.
• SR3-XU: Savannah River (Supplemental Analysis by contract Laboratory) Analysis of sediments for hot acid extractable U. (Exact method undetermined)
• SR3-XX: Savannah River (Supplemental Analysis by contract Laboratory) Analysis of sediments for As, Se, and Ca. (Exact method undetermined)

Water Samples

• SR4: Savannah River Neutron Activation Analysis - Neutron Counting of waters for U.
• SR5: Savannah River Neutron Activation Analysis of waters for Al, Br, Cl, Dy, F, Mn, Na, and V. (Note: Mg may also be reported by this method.)

Discussion of the Reformatting Process for Rocky Mount Quadrangle

Sediment Records
The Rocky Mount quadrangle sediment data consist of reformatted records from the Rocky Mount and Manteo Quadrangles GJBX-16(81) Data Report. These records were compared with corresponding sample records from the North Carolina portion of the North and South Carolina [GJBX-102(82)] Data Report. The following problems were found and addressed during the comparison and reformatting stages for the Rocky Mount quadrangle sediment data:

1. The analytical values for many U, Ce, Dy, Eu, Fe, Lu, and V, determinations differed slightly between the Rocky Mount quadrangle files and the North Carolina State files. These variations are apparently due only to differences in rounding versus truncation of reported values or to differences in the number of recorded significant digits. Since the variation was insignificant, only one set of the values was retained for the affected elements.
2. For some records, analytical values for La and V were found in the North Carolina State files but were missing in the corresponding records from the Rocky Mount quadrangle files. These values were added and that change was noted for each affected record in the REFORMAT comment field.
3. For some records, analytical values for U, Al, Ce, Dy, Eu, Fe, Hf, La, Lu, Th, Ti, V, and Yb were found in the Rocky Mount quadrangle files but were missing in the corresponding records from the North Carolina State files. These missing values were noted for each affected record in the REFORMAT comment field.
4. For 10 records, Rocky Mount quadrangle Neutron Activation Analytical values were significantly different from that found in the corresponding records from the North Carolina State files. For all of these affected records, the differences between Rocky Mount quadrangle files and North and South Carolina State files required the creation of two separate records for each sample to preserve all the data.
5. The date on which a sample was analyzed by Neutron Activation Analysis was only recorded in the State digital data files from the North and South Carolina [GJBX-102(82)] Data Report. This information was added to each of combined sediment data records.
6. During reformatting, contamination codes for "residential" and "recreation" were found to be missing from the state CONTAMC field. These codes were present in the quadrangle format and were added to the final digital data file.
7. An analysis of latitude-longitude site coordinates identified several stream-sediment samples that were missing coordinates, did not plot within expected state, county, or map boundaries, or had differing coordinates in corresponding records. To correct or confirm sample coordinates, the original field collection maps for Lenoir County, North Carolina were obtained and re-digitized. The newly re-digitized coordinates were added to the database and the coordinates from the original file(s) were recorded in the COORDPRB comment field. When the newly re-digitized coordinates were not significantly different, that confirmation of the site location was also noted in the COORDPRB comment field.
8. Gold concentrations from the GJBX-135(82) report were added to the appropriate sediment records. A value of -0.01 (<0.01 ppm Au) was added to all other sediment samples determined to have been analyzed by SRL neutron activation. This value was chosen because 0.01 is the lowest reported gold concentration in the entire report.

Water Records
The Rocky Mount quadrangle water data consist of reformatted records from the Rocky Mount and Manteo Quadrangles GJBX-16(81) Data Report. These records were compared with corresponding sample records from the North Carolina portion of the North and South Carolina [GJBX-102(82)] Data Report. The following problems were found and addressed during the comparison and reformatting stages for the Rocky Mount quadrangle water data:

1. The analytical values for many Al, Br, Dy, and Mn determinations differed slightly between the Rocky Mount quadrangle files and the North Carolina State files. These variations are apparently due only to differences in rounding versus truncation of reported values or to differences in the number of recorded significant digits. Since the variation was insignificant, only one set of the values was retained for the affected elements.
2. For 1 record, the analytical value for Al was found in the North Carolina State files but was missing in the corresponding record from the Rocky Mount quadrangle files. This value was added and that change was noted for each affected record in the REFORMAT comment field.
3. For 540 records, analytical values for Mg were found in the North Carolina State files but were missing in the corresponding records from the Rocky Mount quadrangle files. These values were added and that change was noted for each affected record in the REFORMAT comment field.
4. The original NURE format for surface-water files did not include much information about the character of the sample location. This missing information includes observations taken at each site on the stream width, depth, and flow, water color, surrounding vegetation, local relief, weather, and possible contaminants. This information is given in records for stream-sediment samples that were collected at the same locations. The available site descriptive information for stream-water sites were compared with the corresponding stream-sediment site records. The missing site descriptive data were then added to stream-water records from the corresponding stream-sediment sample records. Sources of data and any problems found are described in the REFORMAT comment field.
5. An analysis of latitude-longitude site coordinates identified several ground-water samples that were missing coordinates, did not plot within expected state, county, or map boundaries, or had differing coordinates in corresponding records. To correct or confirm sample coordinates, the original field collection maps for Edgecombe County, North Carolina Counties, Massachusetts were obtained and re-digitized. The newly re-digitized coordinates were added to the database and the coordinates from the original file(s) were recorded in the COORDPRB comment field. When the newly re-digitized coordinates were not significantly different, that confirmation of the site location was also noted in the COORDPRB comment field.
6. The latitude and longitude coordinates for 1 ground-water sample collected within Beaufort County in North Carolina was not found in the data during the reformatting process. The records for this sample cannot be retrieved on a geographical basis.

Download The Data

The NURE HSSR data are now available online in two databases: The sediment database (also includes data for soils and some rocks) at http://tin.er.usgs.gov/nure/sediment/ and the water database at http://tin.er.usgs.gov/nure/water/. From these two web sites, NURE HSSR data can be selected, examined, summarized, and downloaded by political boundaries (State and County), by quadrangle (1:250,000-scale, 1:100,000-scale, and 1:63,360-scale for Alaska or 1:24,000-scale for the Lower 48 States), and by hydrologic unit (drainage region, subregion, river basin, or sub-basin). Selected data can be downloaded as a dBase file, a shapefile, an HTML table, or ASCII text (tab- or comma-delimited).

Rocky Mount Quadrangle Sediment Data - 512 records
Rocky Mount Quadrangle Water Data - 885 records

Notes for Data Users

In the eastern United States, SRL collected samples primarily by county. Often, not all counties within a quadrangle were completely sampled. Sample coverage in the Rocky Mount quadrangle is complete and includes samples from Beaufort, Bertie, Craven, Duplin, Edgecombe, Greene, Hyde, Jones, Lenoir, Martin, Nash, Pamlico, Pitt, Tyrrell, Washington, Wayne, and Wilson Counties in North Carolina. The laboratory and analytical methods used also may vary by county such that adjacent counties often have very different analytical coverage.

Other NURE Geochemical Data for the Rocky Mount Quadrangle

Geology and Mineral Resources Study
A report on the geology and mineral resources of the Florence, Beaufort, Rocky Mount, and Norfolk quadrangles was prepared for the Savannah River Laboratory [GJBX-197(82)]. No geochemical data accompany this report.

Characteristics of the Southeastern Piedmont
Bendix Field Engineering Corporation released a report that contains stream-sediment, hydrogeochemical, and aeromagnetic data for 16 contiguous NTMS quadrangles in the eastern United States [GJBX-40(83)]. This compilation report is limited in scope to features that have specific interest to the geoscience community. Included in the report are aeromagnetic and geochemical maps, and tectonic and igneous rock distribution maps. When used together, these maps show geochemical, tectonic, and magnetic features unique to many of the geologic and physiographic provinces in the region. This report primarily covers the Southeastern Piedmont region and includes the Athens, Augusta, Bluefield, Charlotte, Florence, Georgetown, Greensboro, Greenville, Knoxville, Norfolk, Raleigh, Richmond, Roanoke, Rocky Mount, Spartanburg and Winston-Salem 1:250,000-scale quadrangles. The color maps are in 35mm-slide format. No digital data files accompany this report.

Rocky Mount Quadrangle NURE Bibliography

• Cook, J.R., 1980, Rocky Mount and Manteo 1° x 2° NTMS areas, North Carolina, data report (abbreviated): E.I. du Pont de Nemours & Co., Savannah River Laboratory, Aiken, S.C., SRL Internal Doc. DPST-80-146-21, U.S. Department of Energy, Grand Junction, Colo., GJBX-16(81), 17 p.
• Fay, W.M., and Cook, J.R., 1982, Gold analyses by neutron activation from SRL NURE samples: E.I. du Pont de Nemours & Co., Savannah River Laboratory, Aiken, S.C., SRL Internal Doc. DPST-81-141-38, U.S. Department of Energy, Grand Junction, Colo., GJBX-135(82), 45 p.
• Harris, W.B., 1982, Geology and mineral resources of the Florence, Beaufort, Rocky Mount, and Norfolk 1° x 2° NTMS quadrangles: E.I. du Pont de Nemours & Co., Savannah River Laboratory, Aiken, S.C., SRL Internal Doc. DPST-81-141-16, U.S. Department of Energy, Grand Junction, Colo., GJBX-197(82), 88 p.
• Madson, M.E., Rush, S.F., Hardy, L.C., LaBonte, N.E., and Ludlam, J.R., 1983, NURE stream-sediment, hydrogeochemical, and aeromagnetic data characteristics of the Piedmont Region, eastern United States: A data release: Bendix Field Engineering Corporation, U.S. Department of Energy, Grand Junction, Colo., GJBX-40(83), 18 p.
• Sargent, K.A., Cook, J.R., and Fay, W.M., 1982, Data report: North and South Carolina: E.I. du Pont de Nemours & Co., Savannah River Laboratory, Aiken, S.C., SRL Internal Doc. DPST-81-146-22, U.S. Department of Energy, Grand Junction, Colo., GJBX-102(82), 45 p.

Links Within Open-File Report 97-492

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Page written by Bryan G. Moravec and Steven M. Smith.
Contact: Steven M. Smith (smsmith@usgs.gov)
Version 1.30: September 11, 2001
Version 1.41: February 23, 2006

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U.S. Department of the Interior | U.S. Geological Survey URL: https://pubsdata.usgs.gov/pubs/of/1997/492/quad/q_rockmt.htm Questions or Assistance: USGS Web Contact Page Last Modified: Wed Dec 7 16:27 EST 2016