USGS Open-File Report 02–94: Water-Quality Data for Pharmaceuticals, Hormones, and Other Organic Wastewater Contaminants in U.S. Streams, 1999-2000

Open-File Report 02–94

Water-Quality Data for Pharmaceuticals, Hormones, and Other Organic Wastewater Contaminants in U.S. Streams, 1999-2000

BY KIMBERLEE K. BARNES, DANA W. KOLPIN, MICHAEL T. MEYER, E. MICHAEL THURMAN, EDWARD T. FURLONG, STEVEN D. ZAUGG, AND LARRY B. BARBER

Table 4. Stream sampling sites analyzed for selected human pharmaceutical compounds (Method 3) in 1999 and 2000
[All concentrations are in micrograms per liter. <, less than indicated detected limit; E, estimated; --, data not collected; Number in parentheses () is the Chemical Abstracts Service Registry Number]

Site code	Date (month-day-year)	Time (24-hour)	Type of sample	Acetaminophen (103-90-2)	Caffeine (58-08-2)	Cimetidine (51481-61-9)	Codeine (76-57-3)	Cotinine (486-56-6)	Dehydronifedipine (67035-22-7)	Digoxigenin (1672-46-4)	Digoxin (20830-75-5)	Diltiazem (42399-41-7)	1,7-Dimethylxanthine (611-59-6)
AR02	05-02-99	1630	regular	--	--	--	--	--	--	--	--	--	--
AR06	05-04-99	2050	do.	--	--	--	--	--	--	--	--	--	--
AZ01	06-29-00	1115	do.	<0.009	3.3	0.016	<.024	0.099	<.01	<0.008	<.26	<.012	0.84
AZ02	06-27-00	1625	do.	.50	1.2	<.007	<.024	.30	.013	<.008	<.26	.037	1.4
AZ03	06-29-00	0710	do.	.048	3.1	.58	<.024	.69	E.003	<.008	<.26	.034	1.8
AZ04	06-27-00	1035	do.	<.009	<.014	<.007	<.024	E.003	<.01	<.008	<.26	.012	.032
CA01	05-18-00	1130	do.	.025	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
CA02	06-28-00	1300	do.	.39	.68	<.007	E.019	<.023	<.01	<.008	<.26	.017	.21
CA03	08-16-00	1700	do.	<.009	.022	<.007	<.024	.071	<.01	<.008	<.26	<.012	<.018
CA04	08-09-00	1700	do.	<.009	<.014	<.007	<.024	<.023	.012	<.008	<.26	<.012	<.018
CA05	04-15-99	1700	do.	<.009	.11	.12	--	.048	.030	<.008	--	<.012	<.018
CA06	04-11-99	0715	do.	--	--	--	--	--	--	--	--	--	--
CA07	09-21-99	1110	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
CA08	09-21-99	1600	do.	E.004	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
CA09	09-22-99	1120	do.	E.004	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
CA10	09-22-99	1320	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
CO01	04-21-99	1250	do.	<.009	<.014	<.007	--	.90	<.01	<.008	--	.049	.053
DE01	05-23-99	1130	do.	--	--	--	--	--	--	--	--	--	--
DE01	05-23-99	1140	duplicate	--	--	--	--	--	--	--	--	--	--
FL01	08-28-00	1215	regular	<.009	.053	<.007	<.024	<.023	<.01	<.008	<.26	<.012	.067
FL02	08-23-00	1215	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
GA01	05-26-99	1400	do.	--	--	--	--	--	--	--	--	--	--
GA02	05-25-99	1130	do.	--	--	--	--	--	--	--	--	--	--
GA03	05-25-99	1030	do.	--	--	--	--	--	--	--	--	--	--
GA04	05-25-99	0840	do.	--	--	--	--	--	--	--	--	--	--
GA05	05-26-99	1130	do.	<.009	.049	<.007	--	E.014	<.01	<.008	--	<.012	<.018
GA06	05-24-99	1215	do.	--	--	--	--	--	--	--	--	--	--
GA07	05-24-99	1420	do.	<.009	E.001	<.007	--	<.023	E.001	<.008	--	E.014	<.018
IA01	09-13-00	1600	do.	<.009	.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
IA02	09-12-00	1200	do.	<.009	.025	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
IA04	09-11-00	1700	do.	<.009	.14	.51	<.024	.024	<.01	<.008	<.26	<.012	.27
IA05	04-05-99	1445	do.	--	--	--	--	--	--	--	--	--	--
IA07	04-08-99	1000	do.	.018	.07	<.007	--	<.023	<.01	<.008	--	<.012	<.018
IA08	04-06-99	0935	do.	--	--	--	--	--	--	--	--	--	--
IA09	04-06-99	1245	do.	--	--	--	--	--	--	--	--	--	--
IA10	04-04-99	2000	do.	--	--	--	--	--	--	--	--	--	--
IA11	04-03-99	1855	do.	--	--	--	--	--	--	--	--	--	--
IA12	04-03-99	1245	do.	--	--	--	--	--	--	--	--	--	--
ID01	08-14-00	1110	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
ID02	08-15-00	1250	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
ID03	08-16-00	1222	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
ID04	05-17-00	1215	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
IL01	05-13-99	1300	do.	<.009	.086	<.007	--	<.023	<.01	<.008	--	<.012	<.018
IL02	05-17-99	1420	do.	--	--	--	--	--	--	--	--	--	--
IL03	05-19-99	1400	do.	<.009	.22	<.007	--	.048	<.01	<.008	--	<.012	<.018
IL04	05-19-99	1240	do.	<.009	.12	<.007	--	.026	<.01	<.008	--	<.012	<.018
IL05	05-20-99	0810	do.	<.009	.056	.053	--	<.023	E.011	<.008	--	E.023	<.018
IL06	05-17-99	1230	do.	--	--	--	--	--	--	--	--	--	--
IL07	05-13-99	1710	do.	--	--	--	--	--	--	--	--	--	--
LA01	04-19-99	1130	do.	<.009	.068	<.007	--	<.023	<.01	<.008	--	<.012	<.018
MA01	05-12-99	0840	do.	<.009	.16	<.007	--	E.011	<.01	<.008	--	<.012	<.018
MA02	07-25-00	0630	do.	<.009	.13	<.007	<.024	E.003	<.01	<.008	<.26	<.012	E.017
MA03	07-25-00	0750	blank	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
MA03	07-25-00	0800	regular	<.009	.085	<.007	<.024	E.018	<.01	<.008	<.26	<.012	<.018
MA03	07-25-00	0810	duplicate	E.007	.067	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
MA04	07-25-00	0900	regular	.40	.74	E.004	<.024	.15	<.01	<.008	<.26	<.012	3.1
MA05	07-25-00	1100	do.	.010	.69	<.007	<.024	E.006	<.01	<.008	<.26	<.012	.26
MA06	07-25-00	1010	do.	.94	2.1	<.007	<.024	.031	<.01	<.008	<.26	E.011	.60
MA07	07-25-00	1130	do.	<.009	.048	<.007	<.024	E.021	<.01	<.008	<.26	<.012	.057
MD01	09-17-99	0930	do.	--	--	--	--	--	--	--	--	--	--
MD02	05-19-99	1710	do.	--	--	--	--	--	--	--	--	--	--
MI01	06-15-99	1030	do.	--	--	--	--	--	--	--	--	--	--
MI02	06-15-99	1430	do.	--	--	--	--	--	--	--	--	--	--
MI03	06-16-99	1045	do.	<.009	<.014	E.012	--	<.023	<.01	<.008	--	<.012	<.018
MN03	10-03-00	1105	blank	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
MN03	10-03-00	1115	do.	<.009	E.002	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
MN04	07-13-99	1300	do.	<.009	E.009	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
MO01	05-06-99	1130	do.	<.009	.75	<.007	--	E.016	<.01	<.008	--	<.012	.097
MO02	04-29-99	1245	do.	10	E6.0	<.007	--	.22	<.01	<.008	--	<.012	1.9
MO03	04-30-99	0830	do.	.24	.68	<.007	<.024	<.023	<.01	<.008	<.26	<.012	.29
MO04	04-30-99	1300	do.	.54	.24	<.007	<.024	<.023	<.01	<.008	<.26	<.012	.13
MO05	05-15-99	1315	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
MO06	04-07-99	0845	do.	--	--	--	--	--	--	--	--	--	--
MO07	04-05-99	1530	do.	--	--	--	--	--	--	--	--	--	--
MO08	04-07-99	0840	do.	<.009	.079	<.007	--	E.02	E.005	<.008	--	<.012	<.018
MT01	03-16-00	1040	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
MT02	03-16-00	1400	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
MT03	03-17-00	1100	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	.061
MT04	03-06-00	1400	do.	<.009	.057	<.007	--	<.023	<.01	<.008	--	<.012	<.018
MT05	03-22-00	1130	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
NC01	05-06-99	1015	do.	--	--	--	--	--	--	--	--	--	--
NC02	05-06-99	1230	do.	--	--	--	--	--	--	--	--	--	--
NC03	05-06-99	1430	do.	--	--	--	--	--	--	--	--	--	--
NC04	05-06-99	1545	do.	--	--	--	--	--	--	--	--	--	--
NC05	05-13-99	1245	do.	--	--	--	--	--	--	--	--	--	--
NE01	06-24-99	1330	do.	--	--	--	--	--	--	--	--	--	--
NE02	06-15-99	1730	do.	--	--	--	--	--	--	--	--	--	--
NE03	06-14-99	1600	do.	--	--	--	--	--	--	--	--	--	--
NE04	06-15-99	1700	do.	--	--	--	--	--	--	--	--	--	--
NE05	06-03-99	1230	do.	--	--	--	--	--	--	--	--	--	--
NE06	06-04-99	1030	do.	--	--	--	--	--	--	--	--	--	--
NE07	06-17-99	1130	do.	--	--	--	--	--	--	--	--	--	--
NJ01	06-01-99	1020	do.	.16	.078	<.007	<.024	E.001	<.01	<.008	<.26	<.012	.045
NJ02	05-27-99	1330	do.	<.009	.033	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NJ03	05-27-99	1550	do.	<.009	E.013	<.007	--	E.019	E.013	<.008	--	<.012	<.018
NJ04	05-27-99	1120	do.	<.009	E.015	.096	--	.039	.020	<.008	--	E.021	<.018
NY01	03-28-00	1310	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
NY02	08-08-00	1150	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY03	08-23-00	1340	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY04	08-08-00	1100	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY05	08-08-00	1300	do.	<.009	.019	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY06	08-08-00	1500	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY07	08-08-00	1410	do.	.059	.23	<.007	<.024	E.002	<.01	<.008	<.26	<.012	<.018
NY07	08-08-00	1415	duplicate	.055	.24	<.007	<.024	E.001	<.01	<.008	<.26	<.012	<.018
NY08	08-30-00	1430	regular	<.009	E.003	<.007	E.009	<.023	<.01	<.008	<.26	<.012	E.01
NY09	08-10-00	1215	do.	<.009	.083	<.007	<.024	<.023	<.01	<.008	<.26	<.012	.021
NY10	08-10-00	1120	do.	.45	E4.7	<.007	<.024	.21	<.01	<.008	<.26	<.012	1.9
NY11	08-10-00	1609	blank	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY11	08-10-00	1625	regular	E9.4	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY12	08-10-00	1515	do.	<.009	.025	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
OH01	05-18-99	1330	do.	.027	.14	<.007	<.024	E.002	<.01	<.008	<.26	<.012	<.018
OH02	05-24-99	1015	do.	--	--	--	--	--	--	--	--	--	--
OH03	05-06-99	1045	do.	--	--	--	--	--	--	--	--	--	--
OH04	05-06-99	1340	do.	--	--	--	--	--	--	--	--	--	--
OH05	05-20-99	1000	do.	<.009	E.006	<.007	--	E.024	<.01	<.008	--	<.012	<.018
OH06	05-24-99	1245	do.	--	--	--	--	--	--	--	--	--	--
OH07	06-02-99	1145	do.	<.009	<.014	<.007	--	.05	.019	<.008	--	.026	<.018
OH08	06-14-99	1120	do.	--	--	--	--	--	--	--	--	--	--
OK01	05-13-99	1315	do.	<.009	.12	<.007	--	E.016	<.01	<.008	--	<.012	<.018
OK03	05-03-99	1045	do.	<.009	.052	<.007	--	<.023	<.01	<.008	--	<.012	<.018
OK04	05-24-99	1300	do.	E.003	<.014	<.007	--	<.023	<.01	<.008	--	E.011	<.018
OR02	07-10-00	1400	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
OR03	06-03-00	1030	do.	<.009	.007	<.007	E.012	<.023	<.01	<.008	<.26	<.012	.048
OR04	07-24-00	1130	do.	<.009	.019	<.007	<.024	<.023	<.01	<.008	<.26	<.012	E.010
PA01	05-24-99	1030	do.	--	--	--	--	--	--	--	--	--	--
PA02	06-08-99	1120	do.	--	--	--	--	--	--	--	--	--	--
PA03	05-27-99	1520	do.	--	--	--	--	--	--	--	--	--	--
PA04	05-27-99	1000	do.	--	--	--	--	--	--	--	--	--	--
PA05	05-27-99	1140	do.	--	--	--	--	--	--	--	--	--	--
TX01	08-09-99	0830	do.	<.009	.05	<.007	--	.059	.027	<.008	--	<.012	<.018
UT01	06-14-99	1230	do.	<.009	<.014	<.007	--	E.017	<.01	<.008	--	<.012	<.018
VA01	08-01-00	1500	do.	E.006	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
WA01	07-19-00	0930	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
WA02	05-18-99	1530	do.	<.009	.13	<.007	--	<.023	<.01	<.008	--	<.012	<.018
WA03	05-14-99	1530	do.	--	--	--	--	--	--	--	--	--	--
WA04	05-06-99	1050	do.	<.009	.17	<.007	--	<.023	<.01	<.008	--	<.012	<.018
WA05	05-14-99	1200	do.	--	--	--	--	--	--	--	--	--	--
WA06	03-29-00	1000	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
WI01	04-23-99	0955	do.	--	--	--	--	--	--	--	--	--	--
WI02	04-23-99	0910	do.	--	--	--	--	--	--	--	--	--	--
WI03	05-17-99	1230	do.	--	--	--	--	--	--	--	--	--	--
WI04	04-23-99	1450	do.	--	--	--	--	--	--	--	--	--	--
WI05	04-23-99	1115	do.	--	--	--	--	--	--	--	--	--	--
WI06	04-23-99	1330	do.	--	--	--	--	--	--	--	--	--	--
WI07	04-23-99	0820	do.	--	--	--	--	--	--	--	--	--	--

Site code

Date (month-day-year)

Time (24-hour)

Type of sample

Acetaminophen (103-90-2)

Caffeine (58-08-2)

Cimetidine (51481-61-9)

Codeine (76-57-3)

Cotinine (486-56-6)

Dehydronifedipine (67035-22-7)

Digoxigenin (1672-46-4)

Digoxin (20830-75-5)

Diltiazem (42399-41-7)

1,7-Dimethylxanthine (611-59-6)

AR02

05-02-99

1630

regular

AR06

05-04-99

2050

do.

AZ01

06-29-00

1115

do.

<0.009

3.3

0.016

<.024

0.099

<.01

<0.008

<.26

<.012

0.84

AZ02

06-27-00

1625

do.

.50

1.2

<.007

<.024

.30

.013

<.008

<.26

.037

1.4

AZ03

06-29-00

0710

do.

.048

3.1

.58

<.024

.69

E.003

<.008

<.26

.034

1.8

AZ04

06-27-00

1035

do.

<.009

<.014

<.007

<.024

E.003

<.01

<.008

<.26

.012

.032

CA01

05-18-00

1130

do.

.025

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

CA02

06-28-00

1300

do.

.39

.68

<.007

E.019

<.023

<.01

<.008

<.26

.017

.21

CA03

08-16-00

1700

do.

<.009

.022

<.007

<.024

.071

<.01

<.008

<.26

<.012

<.018

CA04

08-09-00

1700

do.

<.009

<.014

<.007

<.024

<.023

.012

<.008

<.26

<.012

<.018

CA05

04-15-99

1700

do.

<.009

.11

.12

.048

.030

<.008

<.012

<.018

CA06

04-11-99

0715

do.

CA07

09-21-99

1110

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

CA08

09-21-99

1600

do.

E.004

<.014

<.007

<.023

<.01

<.008

<.012

<.018

CA09

09-22-99

1120

do.

E.004

<.014

<.007

<.023

<.01

<.008

<.012

<.018

CA10

09-22-99

1320

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

CO01

04-21-99

1250

do.

<.009

<.014

<.007

.90

<.01

<.008

.049

.053

DE01

05-23-99

1130

do.

DE01

05-23-99

1140

duplicate

FL01

08-28-00

1215

regular

<.009

.053

<.007

<.024

<.023

<.01

<.008

<.26

<.012

.067

FL02

08-23-00

1215

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

GA01

05-26-99

1400

do.

GA02

05-25-99

1130

do.

GA03

05-25-99

1030

do.

GA04

05-25-99

0840

do.

GA05

05-26-99

1130

do.

<.009

.049

<.007

E.014

<.01

<.008

<.012

<.018

GA06

05-24-99

1215

do.

GA07

05-24-99

1420

do.

<.009

E.001

<.007

<.023

E.001

<.008

E.014

<.018

IA01

09-13-00

1600

do.

<.009

.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

IA02

09-12-00

1200

do.

<.009

.025

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

IA04

09-11-00

1700

do.

<.009

.14

.51

<.024

.024

<.01

<.008

<.26

<.012

.27

IA05

04-05-99

1445

do.

IA07

04-08-99

1000

do.

.018

.07

<.007

<.023

<.01

<.008

<.012

<.018

IA08

04-06-99

0935

do.

IA09

04-06-99

1245

do.

IA10

04-04-99

2000

do.

IA11

04-03-99

1855

do.

IA12

04-03-99

1245

do.

ID01

08-14-00

1110

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

ID02

08-15-00

1250

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

ID03

08-16-00

1222

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

ID04

05-17-00

1215

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

IL01

05-13-99

1300

do.

<.009

.086

<.007

<.023

<.01

<.008

<.012

<.018

IL02

05-17-99

1420

do.

IL03

05-19-99

1400

do.

<.009

.22

<.007

.048

<.01

<.008

<.012

<.018

IL04

05-19-99

1240

do.

<.009

.12

<.007

.026

<.01

<.008

<.012

<.018

IL05

05-20-99

0810

do.

<.009

.056

.053

<.023

E.011

<.008

E.023

<.018

IL06

05-17-99

1230

do.

IL07

05-13-99

1710

do.

LA01

04-19-99

1130

do.

<.009

.068

<.007

<.023

<.01

<.008

<.012

<.018

MA01

05-12-99

0840

do.

<.009

.16

<.007

E.011

<.01

<.008

<.012

<.018

MA02

07-25-00

0630

do.

<.009

.13

<.007

<.024

E.003

<.01

<.008

<.26

<.012

E.017

MA03

07-25-00

0750

blank

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

MA03

07-25-00

0800

regular

<.009

.085

<.007

<.024

E.018

<.01

<.008

<.26

<.012

<.018

MA03

07-25-00

0810

duplicate

E.007

.067

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

MA04

07-25-00

0900

regular

.40

.74

E.004

<.024

.15

<.01

<.008

<.26

<.012

3.1

MA05

07-25-00

1100

do.

.010

.69

<.007

<.024

E.006

<.01

<.008

<.26

<.012

.26

MA06

07-25-00

1010

do.

.94

2.1

<.007

<.024

.031

<.01

<.008

<.26

E.011

.60

MA07

07-25-00

1130

do.

<.009

.048

<.007

<.024

E.021

<.01

<.008

<.26

<.012

.057

MD01

09-17-99

0930

do.

MD02

05-19-99

1710

do.

MI01

06-15-99

1030

do.

MI02

06-15-99

1430

do.

MI03

06-16-99

1045

do.

<.009

<.014

E.012

<.023

<.01

<.008

<.012

<.018

MN03

10-03-00

1105

blank

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

MN03

10-03-00

1115

do.

<.009

E.002

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

MN04

07-13-99

1300

do.

<.009

E.009

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

MO01

05-06-99

1130

do.

<.009

.75

<.007

E.016

<.01

<.008

<.012

.097

MO02

04-29-99

1245

do.

E6.0

<.007

.22

<.01

<.008

<.012

1.9

MO03

04-30-99

0830

do.

.24

.68

<.007

<.024

<.023

<.01

<.008

<.26

<.012

.29

MO04

04-30-99

1300

do.

.54

.24

<.007

<.024

<.023

<.01

<.008

<.26

<.012

.13

MO05

05-15-99

1315

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

MO06

04-07-99

0845

do.

MO07

04-05-99

1530

do.

MO08

04-07-99

0840

do.

<.009

.079

<.007

E.02

E.005

<.008

<.012

<.018

MT01

03-16-00

1040

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

MT02

03-16-00

1400

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

MT03

03-17-00

1100

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

.061

MT04

03-06-00

1400

do.

<.009

.057

<.007

<.023

<.01

<.008

<.012

<.018

MT05

03-22-00

1130

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

NC01

05-06-99

1015

do.

NC02

05-06-99

1230

do.

NC03

05-06-99

1430

do.

NC04

05-06-99

1545

do.

NC05

05-13-99

1245

do.

NE01

06-24-99

1330

do.

NE02

06-15-99

1730

do.

NE03

06-14-99

1600

do.

NE04

06-15-99

1700

do.

NE05

06-03-99

1230

do.

NE06

06-04-99

1030

do.

NE07

06-17-99

1130

do.

NJ01

06-01-99

1020

do.

.16

.078

<.007

<.024

E.001

<.01

<.008

<.26

<.012

.045

NJ02

05-27-99

1330

do.

<.009

.033

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NJ03

05-27-99

1550

do.

<.009

E.013

<.007

E.019

E.013

<.008

<.012

<.018

NJ04

05-27-99

1120

do.

<.009

E.015

.096

.039

.020

<.008

E.021

<.018

NY01

03-28-00

1310

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

NY02

08-08-00

1150

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY03

08-23-00

1340

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY04

08-08-00

1100

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY05

08-08-00

1300

do.

<.009

.019

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY06

08-08-00

1500

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY07

08-08-00

1410

do.

.059

.23

<.007

<.024

E.002

<.01

<.008

<.26

<.012

<.018

NY07

08-08-00

1415

duplicate

.055

.24

<.007

<.024

E.001

<.01

<.008

<.26

<.012

<.018

NY08

08-30-00

1430

regular

<.009

E.003

<.007

E.009

<.023

<.01

<.008

<.26

<.012

E.01

NY09

08-10-00

1215

do.

<.009

.083

<.007

<.024

<.023

<.01

<.008

<.26

<.012

.021

NY10

08-10-00

1120

do.

.45

E4.7

<.007

<.024

.21

<.01

<.008

<.26

<.012

1.9

NY11

08-10-00

1609

blank

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY11

08-10-00

1625

regular

E9.4

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY12

08-10-00

1515

do.

<.009

.025

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

OH01

05-18-99

1330

do.

.027

.14

<.007

<.024

E.002

<.01

<.008

<.26

<.012

<.018

OH02

05-24-99

1015

do.

OH03

05-06-99

1045

do.

OH04

05-06-99

1340

do.

OH05

05-20-99

1000

do.

<.009

E.006

<.007

E.024

<.01

<.008

<.012

<.018

OH06

05-24-99

1245

do.

OH07

06-02-99

1145

do.

<.009

<.014

<.007

.05

.019

<.008

.026

<.018

OH08

06-14-99

1120

do.

OK01

05-13-99

1315

do.

<.009

.12

<.007

E.016

<.01

<.008

<.012

<.018

OK03

05-03-99

1045

do.

<.009

.052

<.007

<.023

<.01

<.008

<.012

<.018

OK04

05-24-99

1300

do.

E.003

<.014

<.007

<.023

<.01

<.008

E.011

<.018

OR02

07-10-00

1400

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

OR03

06-03-00

1030

do.

<.009

.007

<.007

E.012

<.023

<.01

<.008

<.26

<.012

.048

OR04

07-24-00

1130

do.

<.009

.019

<.007

<.024

<.023

<.01

<.008

<.26

<.012

E.010

PA01

05-24-99

1030

do.

PA02

06-08-99

1120

do.

PA03

05-27-99

1520

do.

PA04

05-27-99

1000

do.

PA05

05-27-99

1140

do.

TX01

08-09-99

0830

do.

<.009

.05

<.007

.059

.027

<.008

<.012

<.018

UT01

06-14-99

1230

do.

<.009

<.014

<.007

E.017

<.01

<.008

<.012

<.018

VA01

08-01-00

1500

do.

E.006

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

WA01

07-19-00

0930

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

WA02

05-18-99

1530

do.

<.009

.13

<.007

<.023

<.01

<.008

<.012

<.018

WA03

05-14-99

1530

do.

WA04

05-06-99

1050

do.

<.009

.17

<.007

<.023

<.01

<.008

<.012

<.018

WA05

05-14-99

1200

do.

WA06

03-29-00

1000

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

WI01

04-23-99

0955

do.

WI02

04-23-99

0910

do.

WI03

05-17-99

1230

do.

WI04

04-23-99

1450

do.

WI05

04-23-99

1115

do.

WI06

04-23-99

1330

do.

WI07

04-23-99

0820

do.

Table 4. Selected compounds, Method 3 - Continued

Site code	Date (month-day-year)	Time (24-hour)	Type of sample	Enalaprilat (76420-72-9)	Fluoxetine (54910-89-3)	Gemfibrozil (25812-30-0)	Ibuprofen (15687-27-1)	Metformin (657-24-9)	Paroxetine metabolite	Ranitidine (66357-35-5)	Albuterol (18559-94-9)	Sulfamethoxazole (723-46-6)	Trimethoprim (738-70-5)	Warfarin (81-81-2)
AR02	05-02-99	1630	regular	--	--	--	--	--	--	--	--	--	--	--
AR06	05-04-99	2050	do.	--	--	--	--	--	--	--	--	--	--	--
AZ01	06-29-00	1115	do.	<0.152	<.018	<.015	<.018	<0.003	<.26	<0.01	<0.029	.39	0.20	<.001
AZ02	06-27-00	1625	do.	<.152	<.018	<.015	.36	<.003	<.26	<.01	<.029	.52	.048	<.001
AZ03	06-29-00	0710	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	.35	.11	<.001
AZ04	06-27-00	1035	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	.049	<.014	<.001
CA01	05-18-00	1130	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
CA02	06-28-00	1300	do.	<.152	<.018	.031	.16	<.003	<.26	<.01	<.029	<.023	.030	<.001
CA03	08-16-00	1700	do.	<.152	E.012	<.015	<.018	<.003	<.26	<.01	<.029	.16	<.014	<.001
CA04	08-09-00	1700	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	E.004	<.001
CA05	04-15-99	1700	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	.058	<.001
CA06	04-11-99	0715	do.	--	--	--	--	--	--	--	--	--	--	--
CA07	09-21-99	1110	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
CA08	09-21-99	1600	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
CA09	09-22-99	1120	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
CA10	09-22-99	1320	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
CO01	04-21-99	1250	do.	<.152	<.018	.79	<.018	<.003	<.26	<.01	<.029	<.023	.30	<.001
DE01	05-23-99	1130	do.	--	--	--	--	--	--	--	--	--	--	--
DE01	05-23-99	1140	duplicate	--	--	--	--	--	--	--	--	--	--	--
FL01	08-28-00	1215	regular	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
FL02	08-23-00	1215	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
GA01	05-26-99	1400	do.	--	--	--	--	--	--	--	--	--	--	--
GA02	05-25-99	1130	do.	--	--	--	--	--	--	--	--	--	--	--
GA03	05-25-99	1030	do.	--	--	--	--	--	--	--	--	--	--	--
GA04	05-25-99	0840	do.	--	--	--	--	--	--	--	--	--	--	--
GA05	05-26-99	1130	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
GA06	05-24-99	1215	do.	--	--	--	--	--	--	--	--	--	--	--
GA07	05-24-99	1420	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	.16	.036	<.001
IA01	09-13-00	1600	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	E.004	<.014	<.001
IA02	09-12-00	1200	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
IA04	09-11-00	1700	do.	<.152	<.018	<.015	<.018	<.003	<.26	.014	<.029	.088	.022	<.001
IA05	04-05-99	1445	do.	--	--	--	--	--	--	--	--	--	--	--
IA07	04-08-99	1000	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
IA08	04-06-99	0935	do.	--	--	--	--	--	--	--	--	--	--	--
IA09	04-06-99	1245	do.	--	--	--	--	--	--	--	--	--	--	--
IA10	04-04-99	2000	do.	--	--	--	--	--	--	--	--	--	--	--
IA11	04-03-99	1855	do.	--	--	--	--	--	--	--	--	--	--	--
IA12	04-03-99	1245	do.	--	--	--	--	--	--	--	--	--	--	--
ID01	08-14-00	1110	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
ID02	08-15-00	1250	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
ID03	08-16-00	1222	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
ID04	05-17-00	1215	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
IL01	05-13-99	1300	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
IL02	05-17-99	1420	do.	--	--	--	--	--	--	--	--	--	--	--
IL03	05-19-99	1400	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	E.013	<.001
IL04	05-19-99	1240	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	E.012	<.001
IL05	05-20-99	0810	do.	<.152	<.018	<.015	<.018	.14	<.26	<.01	<.029	.099	.060	<.001
IL06	05-17-99	1230	do.	--	--	--	--	--	--	--	--	--	--	--
IL07	05-13-99	1710	do.	--	--	--	--	--	--	--	--	--	--	--
LA01	04-19-99	1130	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA01	05-12-99	0840	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	E.005	<.001
MA02	07-25-00	0630	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA03	07-25-00	0750	blank	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA03	07-25-00	0800	regular	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA03	07-25-00	0810	duplicate	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA04	07-25-00	0900	regular	<.152	<.018	<.015	.45	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA05	07-25-00	1100	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA06	07-25-00	1010	do.	<.152	<.018	<.015	.10	<.003	<.26	<.01	<.029	<.023	E.001	<.001
MA07	07-25-00	1130	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MD01	09-17-99	0930	do.	--	--	--	--	--	--	--	--	--	--	--
MD02	05-19-99	1710	do.	--	--	--	--	--	--	--	--	--	--	--
MI01	06-15-99	1030	do.	--	--	--	--	--	--	--	--	--	--	--
MI02	06-15-99	1430	do.	--	--	--	--	--	--	--	--	--	--	--
MI03	06-16-99	1045	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	E.011	<.001
MN03	10-03-00	1105	blank	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MN03	10-03-00	1115	regular	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MN04	07-13-99	1300	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	E.009	<.014	<.001
MO01	05-06-99	1130	do.	<.152	<.018	.048	.11	<.003	<.26	<.01	<.029	<.023	E.011	<.001
MO02	04-29-99	1245	do.	<.152	<.018	<.015	1.0	<.003	<.26	<.01	<.029	<.023	E.023	<.001
MO03	04-30-99	0830	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MO04	04-30-99	1300	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MO05	05-15-99	1315	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MO06	04-07-99	0845	do.	--	--	--	--	--	--	--	--	--	--	--
MO07	04-05-99	1530	do.	--	--	--	--	--	--	--	--	--	--	--
MO08	04-07-99	0840	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	E.009	<.001
MT01	03-16-00	1040	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MT02	03-16-00	1400	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MT03	03-17-00	1100	do.	.046	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MT04	03-06-00	1400	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MT05	03-22-00	1130	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NC01	05-06-99	1015	do.	--	--	--	--	--	--	--	--	--	--	--
NC02	05-06-99	1230	do.	--	--	--	--	--	--	--	--	--	--	--
NC03	05-06-99	1430	do.	--	--	--	--	--	--	--	--	--	--	--
NC04	05-06-99	1545	do.	--	--	--	--	--	--	--	--	--	--	--
NC05	05-13-99	1245	do.	--	--	--	--	--	--	--	--	--	--	--
NE01	06-24-99	1330	do.	--	--	--	--	--	--	--	--	--	--	--
NE02	06-15-99	1730	do.	--	--	--	--	--	--	--	--	--	--	--
NE03	06-14-99	1600	do.	--	--	--	--	--	--	--	--	--	--	--
NE04	06-15-99	1700	do.	--	--	--	--	--	--	--	--	--	--	--
NE05	06-03-99	1230	do.	--	--	--	--	--	--	--	--	--	--	--
NE06	06-04-99	1030	do.	--	--	--	--	--	--	--	--	--	--	--
NE07	06-17-99	1130	do.	--	--	--	--	--	--	--	--	--	--	--
NJ01	06-01-99	1020	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NJ02	05-27-99	1330	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NJ03	05-27-99	1550	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NJ04	05-27-99	1120	do.	<.152	<.018	<.015	<.018	.08	<.26	<.01	<.029	<.023	.078	<.001
NY01	03-28-00	1310	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY02	08-08-00	1150	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY03	08-23-00	1340	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY04	08-08-00	1100	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY05	08-08-00	1300	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	E.002	<.014	<.001
NY06	08-08-00	1500	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	E.003	<.014	<.001
NY07	08-08-00	1410	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	.071	E.009	<.001
NY07	08-08-00	1415	duplicate	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	.075	E.009	<.001
NY08	08-30-00	1430	regular	<.152	<.018	<.015	E.032	<.003	<.26	<.01	<.029	.061	E.008	<.001
NY09	08-10-00	1215	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY10	08-10-00	1120	do.	<.152	<.018	<.015	.24	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY11	08-10-00	1609	blank	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY11	08-10-00	1625	regular	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY12	08-10-00	1515	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
OH01	05-18-99	1330	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
OH02	05-24-99	1015	do.	--	--	--	--	--	--	--	--	--	--	--
OH03	05-06-99	1045	do.	--	--	--	--	--	--	--	--	--	--	--
OH04	05-06-99	1340	do.	--	--	--	--	--	--	--	--	--	--	--
OH05	05-20-99	1000	do.	<.152	<.018	<.015	<.018	.042	<.26	<.01	<.029	<.023	E.01	<.001
OH06	05-24-99	1245	do.	--	--	--	--	--	--	--	--	--	--	--
OH07	06-02-99	1145	do.	<.152	<.018	<.015	<.018	0.15	<.26	<.01	<.029	<.023	<.014	<.001
OH08	06-14-99	1120	do.	--	--	--	--	--	--	--	--	--	--	--
OK01	05-13-99	1315	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
OK03	05-03-99	1045	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
OK04	05-24-99	1300	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
OR02	07-10-00	1400	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
OR03	06-03-00	1030	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	.004	E.005	<.001
OR04	07-24-00	1130	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
PA01	05-24-99	1030	do.	--	--	--	--	--	--	--	--	--	--	--
PA02	06-08-99	1120	do.	--	--	--	--	--	--	--	--	--	--	--
PA03	05-27-99	1520	do.	--	--	--	--	--	--	--	--	--	--	--
PA04	05-27-99	1000	do.	--	--	--	--	--	--	--	--	--	--	--
PA05	05-27-99	1150	do.	--	--	--	--	--	--	--	--	--	--	--
TX01	08-09-99	0830	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
UT01	06-14-99	1140	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	E.023	<.014	<.001
VA01	08-01-00	1500	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
WA01	07-19-00	0930	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
WA02	05-18-99	1530	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
WA03	05-14-99	1530	do.	--	--	--	--	--	--	--	--	--	--	--
WA04	05-06-99	1050	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
WA05	05-14-99	1200	do.	--	--	--	--	--	--	--	--	--	--	--
WA06	03-29-00	1000	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
WI01	04-23-99	0955	do.	--	--	--	--	--	--	--	--	--	--	--
WI02	04-23-99	0910	do.	--	--	--	--	--	--	--	--	--	--	--
WI03	05-17-99	1230	do.	--	--	--	--	--	--	--	--	--	--	--
WI04	04-23-99	1450	do.	--	--	--	--	--	--	--	--	--	--	--
WI05	04-23-99	1115	do.	--	--	--	--	--	--	--	--	--	--	--
WI06	04-23-99	1330	do.	--	--	--	--	--	--	--	--	--	--	--
WI07	04-23-99	0820	do.	--	--	--	--	--	--	--	--	--	--	--

Site code

Date (month-day-year)

Time (24-hour)

Type of sample

Enalaprilat (76420-72-9)

Fluoxetine (54910-89-3)

Gemfibrozil (25812-30-0)

Ibuprofen (15687-27-1)

Metformin (657-24-9)

Paroxetine metabolite

Ranitidine (66357-35-5)

Albuterol (18559-94-9)

Sulfamethoxazole (723-46-6)

Trimethoprim (738-70-5)

Warfarin (81-81-2)

AR02

05-02-99

1630

regular

AR06

05-04-99

2050

do.

AZ01

06-29-00

1115

do.

<0.152

<.018

<.015

<.018

<0.003

<.26

<0.01

<0.029

.39

0.20

<.001

AZ02

06-27-00

1625

do.

<.152

<.018

<.015

.36

<.003

<.26

<.01

<.029

.52

.048

<.001

AZ03

06-29-00

0710

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

.35

.11

<.001

AZ04

06-27-00

1035

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

.049

<.014

<.001

CA01

05-18-00

1130

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

CA02

06-28-00

1300

do.

<.152

<.018

.031

.16

<.003

<.26

<.01

<.029

<.023

.030

<.001

CA03

08-16-00

1700

do.

<.152

E.012

<.015

<.018

<.003

<.26

<.01

<.029

.16

<.014

<.001

CA04

08-09-00

1700

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

E.004

<.001

CA05

04-15-99

1700

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

.058

<.001

CA06

04-11-99

0715

do.

CA07

09-21-99

1110

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

CA08

09-21-99

1600

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

CA09

09-22-99

1120

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

CA10

09-22-99

1320

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

CO01

04-21-99

1250

do.

<.152

<.018

.79

<.018

<.003

<.26

<.01

<.029

<.023

.30

<.001

DE01

05-23-99

1130

do.

DE01

05-23-99

1140

duplicate

FL01

08-28-00

1215

regular

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

FL02

08-23-00

1215

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

GA01

05-26-99

1400

do.

GA02

05-25-99

1130

do.

GA03

05-25-99

1030

do.

GA04

05-25-99

0840

do.

GA05

05-26-99

1130

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

GA06

05-24-99

1215

do.

GA07

05-24-99

1420

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

.16

.036

<.001

IA01

09-13-00

1600

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

E.004

<.014

<.001

IA02

09-12-00

1200

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

IA04

09-11-00

1700

do.

<.152

<.018

<.015

<.018

<.003

<.26

.014

<.029

.088

.022

<.001

IA05

04-05-99

1445

do.

IA07

04-08-99

1000

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

IA08

04-06-99

0935

do.

IA09

04-06-99

1245

do.

IA10

04-04-99

2000

do.

IA11

04-03-99

1855

do.

IA12

04-03-99

1245

do.

ID01

08-14-00

1110

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

ID02

08-15-00

1250

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

ID03

08-16-00

1222

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

ID04

05-17-00

1215

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

IL01

05-13-99

1300

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

IL02

05-17-99

1420

do.

IL03

05-19-99

1400

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

E.013

<.001

IL04

05-19-99

1240

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

E.012

<.001

IL05

05-20-99

0810

do.

<.152

<.018

<.015

<.018

.14

<.26

<.01

<.029

.099

.060

<.001

IL06

05-17-99

1230

do.

IL07

05-13-99

1710

do.

LA01

04-19-99

1130

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA01

05-12-99

0840

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

E.005

<.001

MA02

07-25-00

0630

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA03

07-25-00

0750

blank

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA03

07-25-00

0800

regular

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA03

07-25-00

0810

duplicate

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA04

07-25-00

0900

regular

<.152

<.018

<.015

.45

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA05

07-25-00

1100

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA06

07-25-00

1010

do.

<.152

<.018

<.015

.10

<.003

<.26

<.01

<.029

<.023

E.001

<.001

MA07

07-25-00

1130

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MD01

09-17-99

0930

do.

MD02

05-19-99

1710

do.

MI01

06-15-99

1030

do.

MI02

06-15-99

1430

do.

MI03

06-16-99

1045

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

E.011

<.001

MN03

10-03-00

1105

blank

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MN03

10-03-00

1115

regular

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MN04

07-13-99

1300

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

E.009

<.014

<.001

MO01

05-06-99

1130

do.

<.152

<.018

.048

.11

<.003

<.26

<.01

<.029

<.023

E.011

<.001

MO02

04-29-99

1245

do.

<.152

<.018

<.015

1.0

<.003

<.26

<.01

<.029

<.023

E.023

<.001

MO03

04-30-99

0830

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MO04

04-30-99

1300

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MO05

05-15-99

1315

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MO06

04-07-99

0845

do.

MO07

04-05-99

1530

do.

MO08

04-07-99

0840

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

E.009

<.001

MT01

03-16-00

1040

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MT02

03-16-00

1400

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MT03

03-17-00

1100

do.

.046

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MT04

03-06-00

1400

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MT05

03-22-00

1130

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NC01

05-06-99

1015

do.

NC02

05-06-99

1230

do.

NC03

05-06-99

1430

do.

NC04

05-06-99

1545

do.

NC05

05-13-99

1245

do.

NE01

06-24-99

1330

do.

NE02

06-15-99

1730

do.

NE03

06-14-99

1600

do.

NE04

06-15-99

1700

do.

NE05

06-03-99

1230

do.

NE06

06-04-99

1030

do.

NE07

06-17-99

1130

do.

NJ01

06-01-99

1020

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NJ02

05-27-99

1330

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NJ03

05-27-99

1550

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NJ04

05-27-99

1120

do.

<.152

<.018

<.015

<.018

.08

<.26

<.01

<.029

<.023

.078

<.001

NY01

03-28-00

1310

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY02

08-08-00

1150

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY03

08-23-00

1340

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY04

08-08-00

1100

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY05

08-08-00

1300

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

E.002

<.014

<.001

NY06

08-08-00

1500

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

E.003

<.014

<.001

NY07

08-08-00

1410

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

.071

E.009

<.001

NY07

08-08-00

1415

duplicate

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

.075

E.009

<.001

NY08

08-30-00

1430

regular

<.152

<.018

<.015

E.032

<.003

<.26

<.01

<.029

.061

E.008

<.001

NY09

08-10-00

1215

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY10

08-10-00

1120

do.

<.152

<.018

<.015

.24

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY11

08-10-00

1609

blank

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY11

08-10-00

1625

regular

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY12

08-10-00

1515

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

OH01

05-18-99

1330

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

OH02

05-24-99

1015

do.

OH03

05-06-99

1045

do.

OH04

05-06-99

1340

do.

OH05

05-20-99

1000

do.

<.152

<.018

<.015

<.018

.042

<.26

<.01

<.029

<.023

E.01

<.001

OH06

05-24-99

1245

do.

OH07

06-02-99

1145

do.

<.152

<.018

<.015

<.018

0.15

<.26

<.01

<.029

<.023

<.014

<.001

OH08

06-14-99

1120

do.

OK01

05-13-99

1315

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

OK03

05-03-99

1045

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

OK04

05-24-99

1300

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

OR02

07-10-00

1400

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

OR03

06-03-00

1030

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

.004

E.005

<.001

OR04

07-24-00

1130

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

PA01

05-24-99

1030

do.

PA02

06-08-99

1120

do.

PA03

05-27-99

1520

do.

PA04

05-27-99

1000

do.

PA05

05-27-99

1150

do.

TX01

08-09-99

0830

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

UT01

06-14-99

1140

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

E.023

<.014

<.001

VA01

08-01-00

1500

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

WA01

07-19-00

0930

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

WA02

05-18-99

1530

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

WA03

05-14-99

1530

do.

WA04

05-06-99

1050

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

WA05

05-14-99

1200

do.

WA06

03-29-00

1000

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

WI01

04-23-99

0955

do.

WI02

04-23-99

0910

do.

WI03

05-17-99

1230

do.

WI04

04-23-99

1450

do.

WI05

04-23-99

1115

do.

WI06

04-23-99

1330

do.

WI07

04-23-99

0820

do.

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