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Open-File Report 02–94

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Water-Quality Data for Pharmaceuticals, Hormones, and Other Organic Wastewater Contaminants in U.S. Streams, 1999-2000

BY KIMBERLEE K. BARNES, DANA W. KOLPIN, MICHAEL T. MEYER, E. MICHAEL THURMAN, EDWARD T. FURLONG, STEVEN D. ZAUGG, AND LARRY B. BARBER


Table 5. Stream sampling sites analyzed for selected organic wastewater compounds (Method 4) in 1999 and 2000
[All concentrations are in micrograms per liter. <, less than indicated detected limit; E, estimated; --, data not collected; Number in parentheses is the Chemical Abstracts Registry Number] 
Site code Date (month-day-year) Time (24-hour) Type of sample 1,4-dichlorobenzene (106-46-7) 2,6-di-tert-butyl-phenol (128-39-2) 2,6-di-tert-p-benzoquinone (719-22-2) 3-tert-butyl-4-hydroxy anisole (25013-16-5) 4-methyl phenol (106-44-5) 4-nonylphenol(84852-15-3) 4-nonylphenol monoethoxylate   (NA) 4-nonylphenol diethoxylate   (NA)
AR02
05-02-99
1630
regular
--
--
--
--
--
--
--
--
AR06
05-04-99
2050
do.
<0.030
<0.090
0.46
<0.120
<0.030
<.500
<1.000
<1.100
AZ01
06-29-00
1115
do.
<.030
<.080
<.500
<.120
<.060
E4
E2
E2
AZ02
06-27-00
1625
do.
.37
<.080
<.500
<.120
.43
E4
E5
E9
AZ03
06-29-00
0710
do.
.63
<.080
<.500
<.120
<.060
E40
E10
E6
AZ04
06-27-00
1035
do.
.31
<.090
.13
<.120
<.030
E.4
<1.000
<1.100
CA01
05-18-00
1130
do.
<.030
<.090
<.070
<.120
<.030
<.500
<1.000
<1.100
CA02
06-28-00
1300
do.
E.01
<.090
E.04
<.120
<.030
<.500
E.2
E.2
CA03
08-16-00
1700
do.
<.040
<.150
E.4
<.120
E.05
E.7
E2
E4
CA04
08-09-00
1700
do.
.10
<.150
<.500
<.120
.03
E.4
E1
E1
CA05
04-15-99
1700
do.
--
--
--
--
--
--
--
--
CA06
04-11-99
0715
do.
<.030
<.090
<.070
<.120
E.08
<.500
<1.000
<1.100
CA07
09-21-99
1110
do.
<.030
<.090
<.070
<.100
<.030
<.500
<.800
<1.000
CA08
09-21-99
1600
do.
<.030
<.090
<.070
<.100
<.030
<.500
<.800
<1.000
CA09
09-22-99
1120
do.
<.030
<.090
<.070
<.100
<.030
<.500
<.800
<1.000
CA10
09-22-99
1320
do.
<.030
<.090
<.070
<.100
<.030
<.500
<.800
<1.000
CO01
04-21-99
1250
do.
.71
<.090
<.070
E.2
<.030
E10
E20
<1.100
DE01
05-23-99
1130
do.
<.030
<.090
<.070
<.120
<.030
<.500
<1.000
<1.100
DE01
05-23-99
1140
duplicate
<.030
E.04
<.070
<.120
<.030
E.5
E.1
<1.100
FL01
08-28-00
1215
regular
.21
<.150
<.500
<.120
E.04
E.3
E.4
E.8
FL02
08-23-00
1215
do.
<.040
<.150
<.500
<.120
E.04
E.3
E.9
E.4
GA01
05-26-99
1400
do.
--
--
--
--
--
--
--
--
GA02
05-25-99
1130
do.
--
--
--
--
--
--
--
--
GA03
05-25-99
1030
do.
--
--
--
--
--
--
--
--
GA04
05-25-99
0840
do.
<.030
<.090
<.070
<.120
<.030
<.500
E.32
E.4
GA05
05-26-99
1130
do.
--
--
--
--
--
--
--
--
GA06
05-24-99
1215
do.
--
--
--
--
--
--
--
--
GA07
05-31-00
1115
do.
E.02
<.090
<.070
<.120
<.030
<.500
<1.000
E1
IA01
09-13-00
1600
do.
<.030
<.080
<.500
<.120
<.040
E.7
<1.000
<1.100
IA02
09-12-00
1200
do.
<.030
<.080
<.500
<.120
<.060
<.500
<1.000
<1.100
IA04
09-11-00
1700
do.
<.030
<.080
<.500
<.120
<.040
E.9
E1
<1.100
IA05
04-05-99
1445
do.
--
--
--
--
--
--
--
--
IA07
04-08-99
1000
do.
--
--
--
--
--
--
--
--
IA08
04-06-99
0935
do.
--
--
--
--
--
--
--
--
IA09
04-06-99
1245
do.
<.030
<.090
<.070
<.120
E.02
E.6
E.3
E.04
IA10
04-04-99
2000
do.
--
--
--
--
--
--
--
--
IA11
04-03-99
1855
do.
--
--
--
--
--
--
--
--
IA12
04-03-99
1245
do.
--
--
--
--
--
--
--
--
ID01
08-14-00
1110
do.
--
--
--
--
--
--
--
--
ID02
08-15-00
1250
do.
.22
<.150
<.500
<.120
<.060
E.3
<1.000
<1.100
ID03
08-16-00
1222
do.
.26
<.150
<.500
<.120
<.060
E.4
<1.000
<1.100
ID04
05-17-00
1215
do.
<.030
<.090
<.070
<.120
<.030
<.500
<1.000
<1.100
IL01
05-13-99
1300
do.
--
--
--
--
--
--
--
--
IL02
05-17-99
1420
do.
--
--
--
--
--
--
--
--
IL03
09-06-00
1050
do.
<.030
<.080
<.500
<.120
<.040
E.8
<1.000
<1.100
IL04
09-06-00
0940
do.
<.030
<.080
<.500
<.120
<.040
E.8
<1.000
<1.100
IL05
05-20-99
0810
do.
.17
<.090
<.070
<.120
.07
E3
E1
E.7
IL06
05-17-99
1230
do.
--
--
--
--
--
--
--
--
IL07
05-13-99
1710
do.
--
--
--
--
--
--
--
--
LA01
04-19-99
1130
do.
4.3
<.090
<.070
<.120
<.030
E1
<1.000
<1.100
MA01
05-12-99
0840
do.
--
--
--
--
--
--
--
--
MA02
07-25-00
0630
do.
<.030
<.080
<.500
<.120
<.040
<.500
E1
<1.100
MA03
07-25-00
0750
blank
<.030
<.080
<.500
<.120
<.040
<.500
<1.000
<1.100
MA03
07-25-00
0800
regular
<.030
<.080
<.500
<.120
<.040
<.500
E1
<1.100
MA03
07-25-00
0810
duplicate
<.030
<.080
<.500
<.120
<.040
<.500
<1.000
<1.100
MA04
07-25-00
0900
regular
<.030
<.080
<.500
<.120
<.040
<.500
E1
<1.100
MA05
07-25-00
1100
do.
<.030
<.080
<.500
<.120
<.040
<.500
E1
<1.100
MA06
07-25-00
1010
do.
<.030
<.080
<.500
<.120
E.3
<.500
E2
E5
MA07
07-25-00
1130
do.
<.030
<.080
<.500
<.120
<.040
E1
<1.000
<1.100
MD01
09-17-99
0930
do.
--
--
--
--
--
--
--
--
MD02
05-19-99
1710
do.
--
--
--
--
--
--
--
--
MI01
06-15-99
1030
do.
--
--
--
--
--
--
--
--
MI02
06-15-99
1430
do.
--
--
--
--
--
--
--
--
MI03
06-16-99
1045
do.
0.06
E.1
E.06
<.120
<.030
<.500
<1.000
<1.100
MN03
10-03-00
1105
blank
<.040
<.150
<.500
<.120
<.060
E.5
<1.000
<1.100
MN03
10-03-00
1115
regular
<.040
<.150
<.500
<.120
<.060
E.6
<1.000
<1.100
MN04
10-02-00
1210
do.
<.040
<.150
<.500
<.120
E.03
E.5
<1.000
<1.100
MO01
05-06-99
1130
do.
<.030
<.090
<.070
<.120
<.030
E2
E.8
E.6
MO02
04-29-99
1245
do.
E.03
<.090
.14
E.1
.13
E1
E2
E4
MO03
04-30-99
0830
do.
E.03
<.090
<.070
<.120
<.030
E.7
E1
E2
MO04
04-30-99
1300
do.
.09
<.090
<.070
<.120
<.030
E.9
E.7
E1
MO05
05-15-99
1315
do.
<.030
<.090
<.070
<.120
E.02
<.500
<1.000
<1.100
MO06
04-07-99
0845
do.
<.030
<.090
<.070
<.120
<.030
<.500
<1.000
<1.100
MO07
04-05-99
1530
do.
--
--
--
--
--
--
--
--
MO08
04-07-99
0840
do.
--
--
--
--
--
--
--
--
MT01
03-16-00
1040
do.
<.030
<.090
<.070
<.120
<.030
<.500
E1
E.8
MT02
03-16-00
1400
do.
<.030
<.090
<.070
<.120
<.030
E5
E10
E9
MT03
03-17-00
1100
do.
<.030
<.090
<.070
<.120
<.030
E.5
E2
E.7
MT04
03-06-00
1400
do.
<.030
<.090
<.070
<.120
<.030
E1
<1.000
<1.100
MT05
03-22-00
1130
do.
<.030
<.090
<.070
<.120
<.030
<.500
<1.000
<1.100
NC01
05-06-99
1015
do.
--
--
--
--
--
--
--
--
NC02
05-06-99
1230
do.
--
--
--
--
--
--
--
--
NC03
05-06-99
1430
do.
--
--
--
--
--
--
--
--
NC04
05-06-99
1545
do.
--
--
--
--
--
--
--
--
NC05
05-13-99
1245
do.
--
--
--
--
--
--
--
--
NE01
06-24-99
1330
do.
--
--
--
--
--
--
--
--
NE02
06-15-99
1730
do.
<.030
<.090
<.070
<.120
<.030
<.500
<1.000
<1.100
NE03
06-14-99
1600
do.
<.030
E.05
<.070
<.120
<.030
<.500
<1.000
<1.100
NE04
06-15-99
1700
do.
--
--
--
--
--
--
--
--
NE05
06-03-99
1230
do.
--
--
--
--
--
--
--
--
NE06
06-04-99
1030
do.
--
--
--
--
--
--
--
--
NE07
06-17-99
1130
do.
--
--
--
--
--
--
--
--
NJ01
06-01-99
1020
do.
--
--
--
--
--
--
--
--
NJ02
08-15-00
1300
do.
<.030
<.080
<.500
<.120
<.060
E3
E2
<1.100
NJ03
08-17-00
1040
do.
<.040
<.150
<.500
<.120
<.060
E.3
<1.000
<1.100
NJ04
05-27-99
1120
do.
--
--
--
--
--
--
--
--
NY01
03-28-00
1310
do.
<.040
<.150
<.500
<.120
.12
E.4
<1.000
<1.100
NY02
08-08-00
1150
do.
<.040
<.150
<.500
<.120
<.060
<.700
<1.000
<1.100
NY03
08-23-00
1340
do.
<.040
<.150
<.500
<.120
.44
E7
E9
E2
NY04
08-08-00
1100
do.
<.040
<.150
<.500
<.120
<.060
<.700
<1.000
<1.100
NY05
08-08-00
1300
do.
<.040
<.150
<.500
<.120
<.060
E.3
<1.000
<1.100
NY06
08-08-00
1500
do.
<.040
<.150
<.500
<.120
<.060
<.700
<1.000
<1.100
NY07
08-08-00
1410
do.
<.040
<.150
<.500
<.120
E.06
<.700
<1.000
<1.100
NY07
08-08-00
1415
duplicate
<.040
<.150
<.500
<.120
E.05
E.3
E.6
<1.100
NY08
08-30-00
1430
regular
<.030
<.080
<.500
<.120
E.04
E2
E5
E5
NY09
08-10-00
1215
do.
<.040
<.150
<.500
<.120
<.060
E.2
<1.000
E.7
NY10
08-10-00
1120
do.
.06
<.150
<.500
<.120
.06
E6
E8
E8
NY11
08-10-00
1609
blank
<.040
<.150
<.500
<.120
<.060
<.700
<1.000
<1.100
NY11
08-10-00
1625
regular
<.040
<.150
<.500
<.120
<.060
<.700
<1.000
<1.100
NY12
08-10-00
1515
do.
<.040
<.150
<.500
<.120
<.060
E.3
E.6
E.8
OH01
10-05-00
1110
do.
<.040
<.150
<.500
<.120
E.04
E.6
E3
E3
OH02
05-24-99
1015
do.
E.03
<.090
.08
<.120
<.030
E2
E1
E2
OH03
05-06-99
1045
do.
--
--
--
--
--
--
--
--
OH04
05-06-99
1340
do.
--
--
--
--
--
--
--
--
OH05
07-13-00
1130
do.
<.030
<.080
<.500
<.120
<.060
<.500
<1.000
<1.100
OH06
05-24-99
1245
do.
--
--
--
--
--
--
--
--
OH07
06-02-99
1145
do.
--
--
--
--
--
--
--
--
OH08
06-14-99
1120
do.
<.030
E.06
<.070
<.120
<.030
<.500
<1.000
<1.100
OK01
05-13-99
1315
do.
<.030
<.090
<.070
<.120
<.030
E.7
E.07
<1.100
OK03
05-03-99
1045
do.
<.030
<.090
<.070
<.120
<.030
E1
E.5
E.3
OK04
05-24-99
1300
do.
<.030
<.090
<.070
<.120
<.030
<.500
<1.000
<1.100
OR02
07-10-00
1400
do.
<.030
<.090
<.070
<.120
<.030
<.500
<1.000
<1.100
OR03
06-03-00
1030
do.
.06
<.090
<.070
<.120
<.030
<.500
E.5
E.8
OR04
07-24-00
1130
do.
<.030
<.080
<.500
<.120
<.040
E.4
E1
<1.100
PA01
05-24-99
1030
do.
--
--
--
--
--
--
--
--
PA02
06-08-99
1120
do.
--
--
--
--
--
--
--
--
PA03
05-27-99
1520
do.
--
--
--
--
--
--
--
--
PA04
05-27-99
1000
do.
<.030
<.090
<.070
<.120
<.030
E.6
E.2
<1.100
PA05
05-27-99
1150
do.
--
--
--
--
--
--
--
--
TX01
08-09-99
0830
do.
.08
<.090
.22
<.100
<.030
E1
E.9
E.6
UT01
06-14-99
1140
do.
E.01
<.090
<.070
<.120
<.030
<.500
<1.000
<1.100
VA01
08-01-00
1500
do.
<.030
<.080
<.500
<.120
.54
<.500
<1.000
<1.100
WA01
07-19-00
0930
do.
<.030
<.080
<.500
<.120
<.040
<.500
<1.000
<1.100
WA02
05-18-99
1530
do.
--
--
--
--
--
--
--
--
WA03
05-14-99
1530
do.
<.030
<.090
<.070
<.120
<.030
<.500
<1.000
<1.100
WA04
05-06-99
1050
do.
--
--
--
--
--
--
--
--
WA05
05-14-99
1200
do.
--
--
--
--
--
--
--
--
WA06
03-29-00
1000
do.
E.01
<.090
<.070
<.120
E.02
<.500
E.6
E.5
WI01
04-23-99
0955
do.
--
--
--
--
--
--
--
--
WI02
04-23-99
0910
do.
<.030
<.090
<.070
<.120
.04
<.500
<1.000
<1.100
WI03
05-17-99
1230
do.
--
--
--
--
--
--
--
--
WI04
04-23-99
1450
do.
--
--
--
--
--
--
--
--
WI05
04-23-99
1115
do.
--
--
--
--
--
--
--
--
WI06
04-23-99
1330
do.
--
--
--
--
--
--
--
--
WI07
04-23-99
0820
do.
--
--
--
--
--
--
--
--

Table 5. Selected compounds, Method 4 - Continued

Site code Date (month-day-year) Time (24-hour) Type of sample 4-octylphenol monoethoxylate  (26636-32-8) 4-octylphenol diethoxylate  (26636-32-8) 5-methyl-1H-benzo-triazle (136-85-6) Aceto-phenone (98-86-2) Anthra-cene (120-12-7) Benzo (a) pyrene (50-32-8) Bis (2-ethylhexyl) adipate (103-23-1) Bis (2-ethylhexyl) phthalate (117-81-7) Bis-phenol A (80-05-7)
AR02
05-02-99
1630
regular
--
--
--
--
--
--
--
--
--
AR06
05-04-99
2050
do.
<0.100
<0.200
--
<0.100
0.03
E.02
E3
<2.000
<0.090
AZ01
06-29-00
1115
do.
E.1
<.200
.39
<.220
<.060
<.050
<2.000
<2.500
12
AZ02
06-27-00
1625
do.
E.4
E.1
2.4
<.220
<.060
<.050
<2.000
<2.500
5.2
AZ03
06-29-00
0710
do.
E1
<.200
2.1
.28
<.060
<.050
<2.000
<2.500
.40
AZ04
06-27-00
1035
do.
<.100
<.200
.54
<.100
<.050
<.050
<1.500
<2.000
E.06
CA01
05-18-00
1130
do.
<.100
<.200
<.100
<.100
<.050
<.050
<1.500
<2.000
<.090
CA02
06-28-00
1300
do.
<.100
E.003
.10
<.100
<.050
<.050
<1.500
<2.000
<.090
CA03
08-16-00
1700
do.
E.2
E.1
.66
<.220
<.060
<.070
<2.000
<2.500
<.090
CA04
08-09-00
1700
do.
E.3
<.200
.21
<.220
<.060
<.070
<2.000
<2.500
E.08
CA05
04-15-99
1700
do.
--
--
--
--
--
--
--
--
--
CA06
04-11-99
0715
do.
<.100
<.200
--
<.100
<.050
<.050
<1.500
E6
.17
CA07
09-21-99
1110
do.
<.100
<.200
--
<.150
<.050
<.050
<.900
<1.500
E.04
CA08
09-21-99
1600
do.
<.100
<.200
--
<.150
<.050
<.050
<.900
<1.500
<.090
CA09
09-22-99
1120
do.
<.100
<.200
--
<.150
<.050
<.050
<.900
<1.500
E.06
CA10 09-22-99 1320 do. <.100 <.200 -- <.150 <.050 <.050 <.900 <1.500 <.090
CO01 04-21-99 1250 do. E2 E1 -- .41 <.050 <.050 <1.500 E8 E.7
DE01 05-23-99 1130 do. E.1 E.04 -- <.100 <.050 <.050 <1.500 <2.000 <.090
DE01 05-23-99 1140 duplicate <.100 E.04 -- <.100 <.050 <.050 <1.500 E2 <.090
FL01 08-28-00 1215 do. E.09 <.200 <.150 <.220 <.060 <.070 <2.000 <2.000 <.090
FL02 08-23-00 1215 do. E.2 <.200 <.150 <.220 <.060 <.070 <2.000 <2.500 E.09
GA01 05-26-99 1400 do. -- -- -- -- -- -- -- -- --
GA02 05-25-99 1130 do. -- -- -- -- -- -- -- -- --
GA03 05-25-99 1030 do. -- -- -- -- -- -- -- -- --
GA04 05-25-99 0840 do. E.1 E.04 -- <.100 <.060 <.050 E2 E10 E.05
GA05 05-26-99 1130 do. -- -- -- -- -- -- -- -- --
GA06 05-24-99 1215 do. -- -- -- -- -- -- -- -- --
GA07 05-31-00 1115 do. E.1 E.05 <.100 <.100 <.050 <.050 <1.500 <2.000 .23
IA01 09-13-00 1600 do. <.100 <.200 <.100 <.150 <.050 <.050 <2.000 E10 <.090
IA02 09-12-00 1200 do. <.100 <.200 <.100 <.220 <.050 <.050 <2.000 <2.500 <.090
IA04 09-11-00 1700 do. E.06 <.200 <.100 <.150 <.050 <.050 <2.000 <2.500 <.090
IA05 04-05-99 1445 do. -- -- -- -- -- -- -- -- --
IA07 04-08-99 1000 do. -- -- -- -- -- -- -- -- --
IA08 04-06-99 0935 do. -- -- -- -- -- -- -- -- --
IA09 04-06-99 1245 do. E.08 E.03 -- <.100 <.050 <.050 <1.500 E7 E.07
IA10 04-04-99 2000 do. -- -- -- -- -- -- -- -- --
IA11 04-03-99 1855 do. -- -- -- -- -- -- -- -- --
IA12 04-03-99 1245 do. -- -- -- -- -- -- -- -- --
ID01 08-14-00 1110 do. -- -- -- -- -- -- -- -- --
ID02 08-15-00 1250 do. <.120 <.200 <.150 <.220 <.060 <.070 <2.000 <2.500 <.090
ID03 08-16-00 1222 do. E.1 <.200 <.150 <.220 <.060 <.070 <2.000 <2.500 <.090
ID04 05-17-00 1215 do. <.100 <.200 <.100 <.100 <.050 <.050 <1.500 <2.000 <.090
IL01 05-13-99 1300 do. -- -- -- -- -- -- -- -- --
IL02 05-17-99 1420 do. -- -- -- -- -- -- -- -- --
IL03 09-06-00 1050 do. E.06 <.200 .55 <.150 <.050 <.050 <2.000 <2.500 E.8
IL04 09-06-00 0940 do. E.1 <.200 .53 <.150 <.050 E.05 <2.000 E20 E.5
IL05 05-20-99 0810 do. E.3 <.200 -- .10 E.05 .11 <1.500 <2.000 .37
IL06 05-17-99 1230 do. -- -- -- -- -- -- -- -- --
IL07 05-13-99 1710 do. -- -- -- -- -- -- -- -- --
LA01 04-19-99 1130 do. <.100 <.200 -- <.100 <.050 <.050 <1.500 <2.000 E.06
MA01 05-12-99 0840 do. -- -- -- -- -- -- -- -- --
MA02 07-25-00 0630 do. <.100 <.200 <.100 <.150 <.050 <.050 <2.000 <2.500 <.090
MA03 07-25-00 0750 blank <.100 <.200 <.100 <.150 <.050 <.050 <2.000 <2.500 <.090
MA03 07-25-00 0800 regular <.100 <.200 <.100 <.150 <.050 E.03 <2.000 <2.500 <.090
MA03 07-25-00 0810 duplicate <.100 <.200 <.100 <.150 <.050 <.050 <2.000 <2.500 <.090
MA04 07-25-00 0900 regular <.100 <.200 <.100 <.150 <.050 <.050 <2.000 <2.500 <.090
MA05 07-25-00 1100 do. <.100 <.200 <.100 <.150 <.050 <.050 <2.000 <2.500 <.090
MA06 07-25-00 1010 do. <.100 <.200 <.100 <.150 <.050 <.050 <2.000 <2.500 E.08
MA07 07-25-00 1130 do. E.08 <.200 .19 <.150 <.050 <.050 <2.000 <2.500 E.1
MD01 09-17-99 0930 do. -- -- -- -- -- -- -- -- --
MD02 05-19-99 1710 do. -- -- -- -- -- -- -- -- --
MI01 06-15-99 1030 do. -- -- -- -- -- -- -- -- --
MI02 06-15-99 1430 do. -- -- -- -- -- -- -- -- --
MI03 06-16-99 1045 do. <.100 <.200 -- <.100 <.050 <.050 <1.500 <2.000 <.090
MN03 10-03-00 1105 blank E.1 <.200 <.150 <.220 <.060 <.070 <2.000 <2.500 <.090
MN03 10-03-00 1115 regular E.1 <.200 <.150 <.220 <.060 <.070 <2.000 <2.500 <.090
MN04 10-02-00 1210 do. E.2 <.200 .39 <.220 <.060 <.070 <2.000 <2.500 .16
MO01 05-06-99 1130 do. <.100 <.200 -- <.100 <.050 <.050 <1.500 <2.000 E.08
MO02 04-29-99 1245 do. E.3 E.1 -- .15 <.050 <.050 <1.500 E5 .15
MO03 04-30-99 0830 do. E.3 E.09 -- .12 <.050 <.050 <1.500 <2.000 .11
MO04 04-30-99 1300 do. <.100 E.06 -- .15 <.050 <.050 <1.500 <2.000 .12
MO05 05-15-99 1315 do. <.100 <.200 -- <.100 <.050 <.050 <1.500 <2.000 <.090
MO06 04-07-99 0845 do. <.100 <.200 -- <.100 <.050 <.050 <1.500 <2.000 <.090
MO07 04-05-99 1530 do. -- -- -- -- -- -- -- -- --
MO08 04-07-99 0840 do. -- -- -- -- -- -- -- -- --
MT01 03-16-00 1040 do. E.1 E.02 <.100 <.100 <.050 <.050 <1.500 <2.000 <.090
MT02 03-16-00 1400 do. E2 E.25 <.100 <.100 <.050 <.050 <1.500 <2.000 1.1
MT03 03-17-00 1100 do. E.1 <.200 <.100 <.100 <.050 <.050 <1.500 <2.000 <.090
MT04 03-06-00 1400 do. <.100 <.200 <.100 <.100 <.050 <.050 E10 <2.000 .14
MT05 03-22-00 1130 do. <.100 <.200 <.100 <.100 <.050 <.050 <1.500 <2.000 <.090
NC01 05-06-99 1015 do. -- -- -- -- -- -- -- -- --
NC02 05-06-99 1230 do. -- -- -- -- -- -- -- -- --
NC03 05-06-99 1430 do. -- -- -- -- -- -- -- -- --
NC04 05-06-99 1545 do. -- -- -- -- -- -- -- -- --
NC05 05-13-99 1245 do. -- -- -- -- -- -- -- -- --
NE01 06-24-99 1330 do. -- -- -- -- -- -- -- -- --
NE02 06-15-99 1730 do. <.100 <.200 -- <.100 <.050 <.050 <1.500 <2.000 <.090
NE03 06-14-99 1600 do. <.100 <.200 -- .22 <.050 <.050 <1.500 <2.000 .10
NE04 06-15-99 1700 do. -- -- -- -- -- -- -- -- --
NE05 06-03-99 1230 do. -- -- -- -- -- -- -- -- --
NE06 06-04-99 1030 do. -- -- -- -- -- -- -- -- --
NE07 06-17-99 1130 do. -- -- -- -- -- -- -- -- --
NJ01 06-01-99 1020 do. -- -- -- -- -- -- -- -- --
NJ02 08-15-00 1300 do. <.100 <.200 <.100 <.220 .11 <.050 <2.000 <2.500 <.090
NJ03 08-17-00 1040 do. E.1 <.200 .18 <.220 <.060 <.070 <2.000 <2.500 <.090
NJ04 05-27-99 1120 do. -- -- -- -- -- -- -- -- --
NY01 03-28-00 1310 do. <.100 <.200 <.100 <.100 <.060 .22 <1.500 <2.000 <.090
NY02 08-08-00 1150 do. <.120 <.200 <.150 <.220 <.060 E.03 <2.000 <2.500 <.090
NY03 08-23-00 1340 do. E.5 E.1 .19 <.220 <.060 <.070 <2.000 <2.500 .44
NY04 08-08-00 1100 do. <.120 <.200 <.150 <.220 <.060 <.070 <2.000 <2.500 <.090
NY05 08-08-00 1300 do. <.120 <.200 <.150 <.220 <.060 <.070 <2.000 <2.500 <.090
NY06 08-08-00 1500 do. <.120 <.200 <.150 <.220 <.060 <.070 <2.000 <2.500 E.08
NY07 08-08-00 1410 do. <.120 <.200 .17 <.220 <.060 <.070 <2.000 <2.500 <.090
NY07 08-08-00 1415 duplicate <.120 <.200 .25 <.220 <.060 <.070 <2.000 <2.500 E.09
NY08 08-30-00 1430 regular E.2 <.200 <.100 .04 <.050 <.050 <2.000 <2.500 <.090
NY09 08-10-00 1215 do. <.120 <.200 <.150 <.150 <.060 <.070 <2.000 <2.500 <.090
NY10 08-10-00 1120 do. E.6 E.1 .83 <.220 <.060 <.070 <2.000 <2.500 .20
NY11 08-10-00 1609 blank <.120 <.200 <.150 <.220 <.060 <.070 <2.000 <2.500 <.090
NY11 08-10-00 1625 regular E.09 <.200 <.150 <.220 <.060 <.070 <2.000 <2.500 <.090
NY12 08-10-00 1515 do. E.2 <.200 <.150 <.220 <.060 <.070 <2.000 <2.500 <.090
OH01 10-05-00 1110 do. E.8 E.1 .21 <.220 .09 .24 <2.000 <2.500 .22
OH02 05-24-99 1015 do. E.7 E.2 -- <.100 <.050 <.050 <1.500 <2.000 .36
OH03 05-06-99 1045 do. -- -- -- -- -- -- -- -- --
OH04 05-06-99 1340 do. -- -- -- -- -- -- -- -- --
OH05 07-13-00 1130 do. <.100 <.200 <.100 <.220 <.060 E.04 <2.000 <2.500 E.07
OH06 05-24-99 1245 do. -- -- -- -- -- -- -- -- --
OH07 06-02-99 1145 do. -- -- -- -- -- -- -- -- --
OH08 06-14-99 1120 do. <.100 <.200 -- <.100 <.050 <.050 <1.500 <2.000 <.090
OK01 05-13-99 1315 do. <.100 <.200 -- <.100 <.050 <.050 <1.500 <2.000 <.090
OK03 05-03-99 1045 do. <.100 <.200 -- <.100 <.050 <.050 <1.500 <2.000 <.090
OK04 05-24-99 1300 do. <.100 <.200 -- <.100 <.050 <.050 <1.500 <2.000 <.090
OR02 07-10-00 1400 do. <.100 <.200 <.100 <.100 <.050 <.050 <1.500 <2.000 <.090
OR03 06-03-00 1030 do. <.100 <.200 <.100 <.100 <.050 <.050 <1.500 <2.000 <.090
OR04 07-24-00 1130 do. <.100 <.200 <.100 <.150 <.050 <.050 <2.000 <2.500 <.090
PA01 05-24-99 1030 do. -- -- -- -- -- -- -- -- --
PA02 06-08-99 1120 do. -- -- -- -- -- -- -- -- --
PA03 05-27-99 1520 do. -- -- -- -- -- -- -- -- --
PA04 05-27-99 1000 do. E.1 <.200 -- <.100 <.050 <.050 <1.500 E4 <.090
PA05 05-27-99 1150 do. -- -- -- -- -- -- -- -- --
TX01 08-09-99 0830 do. E.4 E.1 -- <.150 <.050 <.050 E.7 E2 <.090
UT01 06-14-99 1140 do. <.100 <.200 -- <.100 <.050 <.050 <1.500 <2.000 <.090
VA01 08-01-00 1500 do. <.100 <.200 <.100 <.220 <.060 <.050 <2.000 <2.500 <.090
WA01 07-19-00 0930 do. <.100 <.200 <.100 <.150 <.050 <.050 <2.000 <2.000 <.090
WA02 05-18-99 1530 do. -- -- -- -- -- -- -- -- --
WA03 05-14-99 1530 do. E.2 E.1 -- <.100 <.050 <.050 <1.500 <2.000 .14
WA04 05-06-99 1050 do. -- -- -- -- -- -- -- -- --
WA05 05-14-99 1200 do. -- -- -- -- -- -- -- -- --
WA06 03-29-00 1000 do. <.100 <.200 .29 E.08 <.050 <.050 <1.500 <2.000 .12
WI01 04-23-99 0955 do. -- -- -- -- -- -- -- -- --
WI02 04-23-99 0910 do. E.1 E.06 -- <.100 <.050 <.050 <1.500 <2.000 <.090
WI03 05-17-99 1230 do. -- -- -- -- -- -- -- -- --
WI04 04-23-99 1450 do. -- -- -- -- -- -- -- -- --
WI05 04-23-99 1115 do. -- -- -- -- -- -- -- -- --
WI06 04-23-99 1330 do. -- -- -- -- -- -- -- -- --
WI07 04-23-99 0820 do. -- -- -- -- -- -- -- -- --

Table 5. Selected compounds, Method 4 - Continued

 
Site code Date (month-day-year) Time (24-hour) Type of sample Butylated hydroxy toluene  (128-37-0) Caffeine (58-08-2) Carbaryl (63-25-2) cis-Chlordane (5103-71-9) Chlor-pyrifos (2921-88-2) Cholesterol (57-88-5) Codeine (76-57-3) Coprostanol (360-68-9) Cotinine (486-56-6) Diazinon (333-41-5)
AR02 05-02-99 1630 regular -- -- -- -- -- -- -- -- -- --
AR06 05-04-99 2050 do. <.080 E0.07 E0.1 <0.040 <0.020 E.7 <.100 E.1 -- .34
AZ01 06-29-00 1115 do. <.080 1.2 <.060 <.040 <.020 <1.500 <.200 E.7 E.03 .25
AZ02 06-27-00 1625 do. <.080 .90 <.060 <.040 <.020 <1.500 <.200 <.600 .20 .27
AZ03 06-29-00 0710 do. <.080 2.6 <.060 <.040 .08 E6 E.7 E3 .57 .35
AZ04 06-27-00 1035 do. <.080 E.05 <.060 <.040 <.020 <1.500 <.100 <.600 .05 <.030
CA01 05-18-00 1130 do. <.080 <.080 <.060 <.040 <.020 <1.500 <.100 <.600 <.040 <.030
CA02 06-28-00 1300 do. <.080 .38 E.01 <.040 E.004 E.1 E.01 E.08 E.02 .04
CA03 08-16-00 1700 do. <.110 .13 E.06 <.040 <.020 <1.500 <.100 <.600 .11 .16
CA04 08-09-00 1700 do. <.110 <.080 <.060 <.040 <.020 <1.500 E.1 E.5 <.080 .07
CA05 04-15-99 1700 do. -- -- -- -- -- -- -- -- -- --
CA06 04-11-99 0715 do. <.080 <.080 <.060 <.040 <.020 E8 <.100 E3 -- <.030
CA07 09-21-99 1110 do. <.080 E.04 E.05 <.040 .04 E.5 <.100 <.600 -- <.030
CA08 09-21-99 1600 do. <.080 E.02 <.060 <.040 .02 E.2 <.100 <.600 -- <.030
CA09 09-22-99 1120 do. <.080 .08 <.060 <.040 <.020 <1.500 <.100 <.600 -- <.030
CA10 09-22-99 1320 do. <.080 <.060 <.060 <.040 .05 E.2 <.100 <.600 -- <.030
CO01 04-21-99 1250 do. E.1 .37 <.060 <.040 <.020 E10 E1 E7 -- <.030
DE01 05-23-99 1130 do. <.080 .08 <.060 <.040 <.020 E.3 <.100 <.600 -- <.030
DE01 05-23-99 1140 duplicate <.080 .09 E.03 <.040 <.020 E.5 <.100 <.600 -- <.030
FL01 08-28-00 1215 regular <.110 .08 <.060 <.040 <.020 <1.500 <.200 <.600 <.080 <.030
FL02 08-23-00 1215 do. <.110 E.06 <.060 <.040 <.020 <1.500 <.200 E.8 <.080 <.030
GA01 05-26-99 1400 do. -- -- -- -- -- -- -- -- -- --
GA02 05-25-99 1130 do. -- -- -- -- -- -- -- -- -- --
GA03 05-25-99 1030 do. -- -- -- -- -- -- -- -- -- --
GA04 05-25-99 0840 do. <.080 E.07 <.060 <.040 <.020 E3 <.100 <.600 -- <.030
GA05 05-26-99 1130 do. -- -- -- -- -- -- -- -- -- --
GA06 05-24-99 1215 do. -- -- -- -- -- -- -- -- -- --
GA07 05-31-00 1115 do. <.080 .09 <.060 <.040 <.020 E4 <.100 E.7 <.040 .04
IA01 09-13-00 1600 do. <.080 <.080 <.060 <.040 <.020 <1.500 <.100 <.600 <.040 <.030
IA02 09-12-00 1200 do. <.080 <.080 <.060 <.040 <.020 <1.500 <.100 <.600 <.040 <.030
IA04 09-11-00 1700 do. <.080 .16 <.060 <.040 <.020 E2 <.100 E1 E.04 <.030
IA05 04-05-99 1445 do. -- -- -- -- -- -- -- -- -- --
IA07 04-08-99 1000 do. -- -- -- -- -- -- -- -- -- --
IA08 04-06-99 0935 do. -- -- -- -- -- -- -- -- -- --
IA09 04-06-99 1245 do. <.080 .12 <.060 <.040 <.020 E.4 <.100 <.600 -- <.030
IA10 04-04-99 2000 do. -- -- -- -- -- -- -- -- -- --
IA11 04-03-99 1855 do. -- -- -- -- -- -- -- -- -- --
IA12 04-03-99 1245 do. -- -- -- -- -- -- -- -- -- --
ID01 08-14-00 1110 do. -- -- -- -- -- -- -- -- -- --
ID02 08-15-00 1250 do. <.110 <.080 <.060 <.040 <.020 <1.500 <.200 <.600 <.080 E.02
ID03 08-16-00 1222 do. <.110 <.080 <.060 <.040 .03 <1.500 <.200 <.600 <.080 <.030
ID04 05-17-00 1215 do. <.080 <.080 <.060 <.040 <.020 <1.500 <.100 <.600 <.040 <.030
IL01 05-13-99 1300 do. -- -- -- -- -- -- -- -- -- --
IL02 05-17-99 1420 do. -- -- -- -- -- -- -- -- -- --
IL03 09-06-00 1050 do. <.080 .14 <.060 <.040 <.020 <1.500 <.100 <.600 .05 <.030
IL04 09-06-00 0940 do. <.080 .10 <.060 <.040 <.020 <1.500 <.100 <.600 .05 <.030
IL05 05-20-99 0810 do. <.080 .30 <.060 <.040 <.020 E1 <.100 E.5 -- .28
IL06 05-17-99 1230 do. -- -- -- -- -- -- -- -- -- --
IL07 05-13-99 1710 do. -- -- -- -- -- -- -- -- -- --
LA01 04-19-99 1130 do. <.080 E.08 <.060 <.040 <.020 E.1 <.100 <.600 -- <.030
MA01 05-12-99 0840 do. -- -- -- -- -- -- -- -- -- --
MA02 07-25-00 0630 do. <.080 .10 E.02 E.001 <.020 E1 <.100 <.600 E.01 .04
MA03 07-25-00 0750 blank <.080 <.080 <.060 <.040 <.020 <1.500 <.100 <.600 <.040 <.030
MA03 07-25-00 0800 regular <.080 .49 E.02 <.040 <.020 E2 <.100 E1 <.040 <.030
MA03 07-25-00 0810 duplicate <.080 E.07 E.03 E.002 <.020 <1.500 <.100 <.600 <.040 .20
MA04 07-25-00 0900 regular <.080 .46 <.060 <.040 <.020 E3 <.100 E1 .07 E.03
MA05 07-25-00 1100 do. <.080 E.07 E.03 E.002 <.020 <1.500 <.100 <.600 <.040 .22
MA06 07-25-00 1010 do. <.080 1.6 <.060 <.040 <.020 E2 <.100 E1 .04 <.030
MA07 07-25-00 1130 do. <.080 .15 E.05 <.040 <.020 <1.500 <.100 <.600 .06 .06
MD01 09-17-99 0930 do. -- -- -- -- -- -- -- -- -- --
MD02 05-19-99 1710 do. -- -- -- -- -- -- -- -- -- --
MI01 06-15-99 1030 do. -- -- -- -- -- -- -- -- -- --
MI02 06-15-99 1430 do. -- -- -- -- -- -- -- -- -- --
MI03 06-16-99 1045 do. E.1 <.080 <.060 <.040 <.020 <1.500 <.100 <.600 -- <.030
MN03 10-03-00 1105 blank <.110 <.080 <.060 <.040 <.020 <1.500 <.200 <.600 <.080 <.030
MN03 10-03-00 1115 regular <.110 E.04 <.060 <.040 <.020 <1.500 <.200 <.600 <.080 <.030
MN04 10-02-00 1210 do. <.110 .10 <.060 <.040 <.020 E2 <.200 <.600 E.05 <.030
MO01 05-06-99 1130 do. <.080 .99 E.008 <.040 .06 E2 <.100 E.7 -- .06
MO02 04-29-99 1245 do. <.080 4.2 <.060 .10 .11 <1.000 <.100 E10 -- <.030
MO03 04-30-99 0830 do. <.080 4.0 <.060 <.040 .06 E10 E.2 E8 -- <.030
MO04 04-30-99 1300 do. <.080 2.6 <.060 .04 .09 E2 E.2 E.7 -- .07
MO05 05-15-99 1315 do. <.080 <.080 <.060 <.040 <.020 <1.000 <.100 <.600 -- <.030
MO06 04-07-99 0845 do. <.080 .03 <.060 <.040 <.020 E.07 <.100 <.600 -- <.030
MO07 04-05-99 1530 do. -- -- -- -- -- -- -- -- -- --
MO08 04-07-99 0840 do. -- -- -- -- -- -- -- -- -- --
MT01 03-16-00 1040 do. <.080 .10 <.060 <.040 <.020 <1.500 <.100 <.600 <.040 <.030
MT02 03-16-00 1400 do. <.080 .97 <.060 <.040 <.020 E1 <.100 E3 <.040 <.030
MT03 03-17-00 1100 do. <.080 E.07 <.060 <.040 .19 <1.500 <.100 <.600 <.040 <.030
MT04 03-06-00 1400 do. <.080 .19 <.060 <.040 <.020 E3 <.100 <.600 <.040 <.030
MT05 03-22-00 1130 do. <.080 E.04 <.060 <.040 <.020 E1 <.100 E.3 <.040 <.030
NC01 05-06-99 1015 do. -- -- -- -- -- -- -- -- -- --
NC02 05-06-99 1230 do. -- -- -- -- -- -- -- -- -- --
NC03 05-06-99 1430 do. -- -- -- -- -- -- -- -- -- --
NC04 05-06-99 1545 do. -- -- -- -- -- -- -- -- -- --
NC05 05-13-99 1245 do. -- -- -- -- -- -- -- -- -- --
NE01 06-24-99 1330 do. -- -- -- -- -- -- -- -- -- --
NE02 06-15-99 1730 do. <.080 <.080 <.060 <.040 <.020 E.6 <.100 <.600 -- <.030
NE03 06-14-99 1600 do. <.080 <.080 <.060 <.040 <.020 E3 <.100 E.6 -- <.030
NE04 06-15-99 1700 do. -- -- -- -- -- -- -- -- -- --
NE05 06-03-99 1230 do. -- -- -- -- -- -- -- -- -- --
NE06 06-04-99 1030 do. -- -- -- -- -- -- -- -- -- --
NE07 06-17-99 1130 do. -- -- -- -- -- -- -- -- -- --
NJ01 06-01-99 1020 do. -- -- -- -- -- -- -- -- -- --
NJ02 08-15-00 1300 do. <.080 .15 E.08 <.040 <.020 <1.500 <.200 <.600 E.005 .11
NJ03 08-17-00 1040 do. <.110 .08 E.04 <.040 <.020 <1.500 <.200 <.600 <.080 .09
NJ04 05-27-99 1120 do. -- -- -- -- -- -- -- -- -- --
NY01 03-28-00 1310 do. <.080 E.06 <.060 <.040 <.020 E3 <.100 E.4 <.040 <.030
NY02 08-08-00 1150 do. <.110 <.080 <.060 <.040 <.020 <1.500 <.200 <.600 <.080 <.030
NY03 08-23-00 1340 do. <.110 1.6 <.060 <.040 .31 E9 <.200 E9 <.080 <.030
NY04 08-08-00 1100 do. <.110 <.080 <.060 <.040 <.020 E2 <.200 <.600 <.080 <.030
NY05 08-08-00 1300 do. <.110 E.05 <.060 <.040 <.020 <1.500 <.200 <.600 <.080 <.030
NY06 08-08-00 1500 do. <.110 <.080 <.060 <.040 <.020 <1.500 <.200 <.600 <.080 <.030
NY07 08-08-00 1410 do. <.110 .37 <.060 <.040 <.020 <1.500 <.200 <.600 <.080 <.030
NY07 08-08-00 1415 duplicate <.110 .32 <.060 <.040 <.020 <1.500 <.200 <.600 <.080 <.030
NY08 08-30-00 1430 regular <.080 <.080 <.060 <.040 .08 <1.500 <.100 <.600 .05 <.030
NY09 08-10-00 1215 do. <.110 E.07 <.060 <.040 <.020 <1.500 <.200 <.600 <.080 <.030
NY10 08-10-00 1120 do. <.110 5.7 <.060 <.040 <.020 E2 <.200 E2 .16 <.030
NY11 08-10-00 1609 blank <.110 <.080 <.060 <.040 <.020 <1.500 <.200 <.600 <.080 <.030
NY11 08-10-00 1625 regular <.110 <.080 E.1 <.040 <.020 <1.500 <.200 <.600 <.080 <.030
NY12 08-10-00 1515 do. <.110 E.05 <.060 <.040 <.020 <1.500 <.200 <.600 <.080 <.030
OH01 10-05-00 1110 do. <.110 .18 <.060 <.040 <.020 E1 <.200 E1 <.080 .12
OH02 05-24-99 1015 do. <.080 .53 <.060 <.040 <.020 E.7 <.200 E.2 -- .07
OH03 05-06-99 1045 do. -- -- -- -- -- -- -- -- -- --
OH04 05-06-99 1340 do. -- -- -- -- -- -- -- -- -- --
OH05 07-13-00 1130 do. <.080 E.04 <.060 <.040 <.020 <1.500 <.200 <.600 <.040 .05
OH06 05-24-99 1245 do. -- -- -- -- -- -- -- -- -- --
OH07 06-02-99 1145 do. -- -- -- -- -- -- -- -- -- --
OH08 06-14-99 1120 do. <.080 E.07 E.04 <.040 <.020 E.8 <.100 <.600 -- <.030
OK01 05-13-99 1315 do. <.080 .18 <.060 <.040 <.020 E.3 <.100 E.1 -- E.01
OK03 05-03-99 1045 do. <.080 <.080 <.060 <.040 <.020 E.4 <.100 E.2 -- <.030
OK04 05-24-99 1300 do. <.080 <.080 <.060 <.040 <.020 E.2 <.100 <.600 -- <.030
OR02 07-10-00 1400 do. <.080 <.080 <.060 <.040 <.020 <1.500 <.100 <.600 <.040 <.030
OR03 06-03-00 1030 do. <.080 E.03 <.060 <.040 <.020 E2 <.100 <.600 <.040 <.030
OR04 07-24-00 1130 do. <.080 <.080 <.060 <.040 <.020 E1 <.100 <.600 <.040 <.030
PA01 05-24-99 1030 do. -- -- -- -- -- -- -- -- -- --
PA02 06-08-99 1120 do. -- -- -- -- -- -- -- -- -- --
PA03 05-27-99 1520 do. -- -- -- -- -- -- -- -- -- --
PA04 05-27-99 1000 do. <.080 E.06 <.060 <.040 <.020 E.3 <.100 <.600 -- <.030
PA05 05-27-99 1150 do. -- -- -- -- -- -- -- -- -- --
TX01 08-09-99 0830 do. <.080 .17 <.060 <.040 <.020 E2 <.100 E.4 -- <.030
UT01 06-14-99 1140 do. <.080 E.03 <.060 <.040 <.020 E.1 <.100 <.600 -- <.030
VA01 08-01-00 1500 do. <.080 .09 <.060 <.040 <.020 <1.500 <.200 <.600 <.040 <.030
WA01 07-19-00 0930 do. <.080 <.080 E.01 <.040 <.020 E1 <.100 <.600 <.040 <.030
WA02 05-18-99 1530 do. -- -- -- -- -- -- -- -- -- --
WA03 05-14-99 1530 do. <.080 E.04 <.060 <.040 <.020 <1.000 <.100 <.600 -- <.030
WA04 05-06-99 1050 do. -- -- -- -- -- -- -- -- -- --
WA05 05-14-99 1200 do. -- -- -- -- -- -- -- -- -- --
WA06 03-29-00 1000 do. <.080 <.080 <.060 <.040 <.020 E.5 <.100 <.600 <.040 <.030
WI01 04-23-99 0955 do. -- -- -- -- -- -- -- -- -- --
WI02 04-23-99 0910 do. <.080 <.080 <.060 <.040 <.020 E.8 <.100 E.1 -- <.030
WI03 05-17-99 1230 do. -- -- -- -- -- -- -- -- -- --
WI04 04-23-99 1450 do. -- -- -- -- -- -- -- -- -- --
WI05 04-23-99 1115 do. -- -- -- -- -- -- -- -- -- --
WI06 04-23-99 1330 do. -- -- -- -- -- -- -- -- -- --
WI07 04-23-99 0820 do. -- -- -- -- -- -- -- -- -- --
Table 5. Selected compounds, Method 4 - Continued

 
Site code Date (month-day-year) Time (24-hour) Type of sample Dieldrin (60-57-1) Diethyl-phthalate (84-66-2) N,N-di-ethyl-toluamide (134-62-3) 17b-estradiol (50-28-2) Ethanol, 2-butoxy phosphate (78-51-3) Fluoranthene (206-44-0) Lindane (58-89-9) Methyl parathion (298-00-0) Naphthalene (91-20-3) Phenanthrene (85-01-8)
AR02 05-02-99 1630 regular -- -- -- -- -- -- -- -- -- --
AR06 05-04-99 2050 do. <0.080 -- -- <.500 0.14 0.22 <.050 <0.060 0.06 0.14
AZ01 06-29-00 1115 do. <.080 <.250 .51 <.500 .69 <.030 <.050 <.060 <.020 <.050
AZ02 06-27-00 1625 do. <.080 E.2 .50 <.500 6.7 <.030 <.050 <.060 <.020 <.050
AZ03 06-29-00 0710 do. <.080 E.2 1.1 <.500 <.200 <.030 <.050 <.060 <.020 <.050
AZ04 06-27-00 1035 do. <.080 <.250 .05 <.500 .55 <.030 <.050 <.060 <.030 <.060
CA01 05-18-00 1130 do. <.080 <.250 <.040 <.500 <.070 <.030 <.050 <.060 <.030 <.060
CA02 06-28-00 1300 do. <.080 <.250 .06 <.500 .08 <.030 E.01 E.01 <.030 <.060
CA03 08-16-00 1700 do. <.080 <.350 .19 <.500 <.200 <.030 .11 <.060 <.025 <.050
CA04 08-09-00 1700 do. <.080 <.350 .10 E.1 <.200 <.030 E.02 <.060 .03 <.050
CA05 04-15-99 1700 do. -- -- -- -- -- -- -- -- -- --
CA06 04-11-99 0715 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
CA07 09-21-99 1110 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
CA08 09-21-99 1600 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
CA09 09-22-99 1120 do. <.080 -- -- <.500 <.070 E.02 <.050 <.060 <.030 <.060
CA10 09-22-99 1320 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
CO01 04-21-99 1250 do. <.080 -- -- <.500 5.4 <.030 <.050 <.060 <.030 <.060
DE01 05-23-99 1130 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
DE01 05-23-99 1140 duplicate <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
FL01 08-28-00 1215 regular <.080 <.350 .40 <.500 <.200 <.030 E.02 <.060 <.025 <.050
FL02 08-23-00 1215 do. <.080 <.350 <.080 E.1 .29 <.030 <.050 <.060 <.025 <.050
GA01 05-26-99 1400 do. -- -- -- -- -- -- -- -- -- --
GA02 05-25-99 1130 do. -- -- -- -- -- -- -- -- -- --
GA03 05-25-99 1030 do. -- -- -- -- -- -- -- -- -- --
GA04 05-25-99 0840 do. <.080 -- -- <.500 .65 <.030 <.050 <.060 <.030 <.060
GA05 05-26-99 1130 do. -- -- -- -- -- -- -- -- -- --
GA06 05-24-99 1215 do. -- -- -- -- -- -- -- -- -- --
GA07 05-31-00 1115 do. <.080 <.250 .09 E.1 .30 .04 <.050 <.060 <.030 <.060
IA01 09-13-00 1600 do. <.080 <.250 E.04 <.500 <.200 E.005 <.050 <.060 <.020 <.060
IA02 09-12-00 1200 do. <.080 <.250 E.04 <.500 <.200 <.030 <.050 <.060 <.020 <.060
IA04 09-11-00 1700 do. <.080 <.250 .07 <.500 .42 E.006 <.050 <.060 <.020 <.060
IA05 04-05-99 1445 do. -- -- -- -- -- -- -- -- -- --
IA07 04-08-99 1000 do. -- -- -- -- -- -- -- -- -- --
IA08 04-06-99 0935 do. -- -- -- -- -- -- -- -- -- --
IA09 04-06-99 1245 do. <.080 -- -- <.500 .48 <.030 <.050 <.060 <.030 <.060
IA10 04-04-99 2000 do. -- -- -- -- -- -- -- -- -- --
IA11 04-03-99 1855 do. -- -- -- -- -- -- -- -- -- --
IA12 04-03-99 1245 do. -- -- -- -- -- -- -- -- -- --
ID01 08-14-00 1110 do. -- -- -- -- -- -- -- -- -- --
ID02 08-15-00 1250 do. <.080 <.350 <.080 <.500 <.070 <.030 <.050 <.060 <.025 <.050
ID03 08-16-00 1222 do. <.080 <.350 <.080 <.500 <.070 <.030 <.050 <.060 <.025 <.050
ID04 05-17-00 1215 do. <.080 <.250 <.040 <.500 <.070 <.030 <.050 <.060 <.030 <.060
IL01 05-13-99 1300 do. -- -- -- -- -- -- -- -- -- --
IL02 05-17-99 1420 do. -- -- -- -- -- -- -- -- -- --
IL03 09-06-00 1050 do. <.080 E.2 .24 <.500 .24 E.08 <.050 <.060 <.020 E.02
IL04 09-06-00 0940 do. <.080 <.250 .09 <.500 <.200 E.2 <.050 <.060 <.020 E.04
IL05 05-20-99 0810 do. <.080 -- -- <.500 .82 .20 <.050 <.060 E.02 .06
IL06 05-17-99 1230 do. -- -- -- -- -- -- -- -- -- --
IL07 05-13-99 1710 do. -- -- -- -- -- -- -- -- -- --
LA01 04-19-99 1130 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
MA01 05-12-99 0840 do. -- -- -- -- -- -- -- -- -- --
MA02 07-25-00 0630 do. <.080 <.250 .05 <.500 .22 <.030 <.050 <.060 <.020 <.060
MA03 07-25-00 0750 blank <.080 <.250 <.040 <.500 <.200 <.030 <.050 <.060 E.02 <.060
MA03 07-25-00 0800 regular <.080 <.250 .08 <.500 .31 <.030 <.050 <.060 E.02 <.060
MA03 07-25-00 0810 duplicate <.080 <.250 .04 <.500 .38 <.030 <.050 <.060 E.02 <.060
MA04 07-25-00 0900 regular <.080 <.250 .10 <.500 <.200 <.030 <.050 <.060 <.020 <.060
MA05 07-25-00 1100 do. <.080 <.250 .05 <.500 .51 <.030 <.050 <.060 <.020 <.060
MA06 07-25-00 1010 do. <.080 <.250 .08 <.500 .49 <.030 <.050 <.060 E.03 <.060
MA07 07-25-00 1130 do. <.080 E.2 .09 <.500 .62 E.04 <.050 <.060 <.030 <.060
MD01 09-17-99 0930 do. -- -- -- -- -- -- -- -- -- --
MD02 05-19-99 1710 do. -- -- -- -- -- -- -- -- -- --
MI01 06-15-99 1030 do. -- -- -- -- -- -- -- -- -- --
MI02 06-15-99 1430 do. -- -- -- -- -- -- -- -- -- --
MI03 06-16-99 1045 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
MN03 10-03-00 1105 blank <.080 <.350 <.080 <.500 E.2 <.030 <.050 <.060 .02 <.050
MN03 10-03-00 1115 regular <.080 <.350 <.080 <.500 <.200 <.030 <.050 <.060 <.025 <.050
MN04 10-02-00 1210 do. <.080 <.350 E.06 <.500 .63 <.030 <.050 <.060 <.025 <.050
MO01 05-06-99 1130 do. <.080 -- -- <.500 1.4 .07 <.050 <.060 <.030 <.060
MO02 04-29-99 1245 do. .21 -- -- <.500 2.0 <.030 <.050 <.060 E.02 <.060
MO03 04-30-99 0830 do. .21 -- -- <.500 2.3 <.030 <.050 <.060 <.030 <.060
MO04 04-30-99 1300 do. .15 -- -- <.500 1.4 .1 <.050 <.060 <.030 <.060
MO05 05-15-99 1315 do. <.080 -- -- <.500 <.070 E.03 <.050 <.060 <.030 <.060
MO06 04-07-99 0845 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
MO07 04-05-99 1530 do. -- -- -- -- -- -- -- -- -- --
MO08 04-07-99 0840 do. -- -- -- -- -- -- -- -- -- --
MT01 03-16-00 1040 do. <.080 <.250 <.040 <.500 <.070 <.030 <.050 <.060 <.030 <.060
MT02 03-16-00 1400 do. <.080 .36 .55 E.2 3.8 <.030 <.050 <.060 <.030 <.060
MT03 03-17-00 1100 do. <.080 <.250 E.03 <.500 .23 <.030 <.050 <.060 <.030 <.060
MT04 03-06-00 1400 do. <.080 .42 .19 <.500 <.070 <.030 <.050 <.060 .07 E.04
MT05 03-22-00 1130 do. <.080 <.250 E.04 <.500 <.070 <.030 <.050 <.060 <.030 <.060
NC01 05-06-99 1015 do. -- -- -- -- -- -- -- -- -- --
NC02 05-06-99 1230 do. -- -- -- -- -- -- -- -- -- --
NC03 05-06-99 1430 do. -- -- -- -- -- -- -- -- -- --
NC04 05-06-99 1545 do. -- -- -- -- -- -- -- -- -- --
NC05 05-13-99 1245 do. -- -- -- -- -- -- -- -- -- --
NE01 06-24-99 1330 do. -- -- -- -- -- -- -- -- -- --
NE02 06-15-99 1730 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
NE03 06-14-99 1600 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
NE04 06-15-99 1700 do. -- -- -- -- -- -- -- -- -- --
NE05 06-03-99 1230 do. -- -- -- -- -- -- -- -- -- --
NE06 06-04-99 1030 do. -- -- -- -- -- -- -- -- -- --
NE07 06-17-99 1130 do. -- -- -- -- -- -- -- -- -- --
NJ01 06-01-99 1020 do. -- -- -- -- -- -- -- -- -- --
NJ02 08-15-00 1300 do. <.080 <.250 E.03 <.500 E.1 E.02 <.050 <.060 E.02 <.050
NJ03 08-17-00 1040 do. <.080 <.350 E.05 <.500 E.2 <.030 <.050 <.060 <.025 <.050
NJ04 05-27-99 1120 do. -- -- -- -- -- -- -- -- -- --
NY01 03-28-00 1310 do. <.080 <.250 .06 <.500 <.070 .13 <.050 <.060 <.030 E.04
NY02 08-08-00 1150 do. <.080 <.350 <.080 <.500 <.200 .09 <.050 <.060 <.025 E.03
NY03 08-23-00 1340 do. <.080 <.350 .24 E.2 1.0 <.030 <.050 <.060 <.025 <.060
NY04 08-08-00 1100 do. <.080 <.350 E.05 <.500 <.200 <.030 <.050 <.060 <.025 <.050
NY05 08-08-00 1300 do. <.080 <.350 E.05 <.500 <.200 .06 <.050 <.060 <.025 <.050
NY06 08-08-00 1500 do. <.080 <.350 <.080 <.500 <.200 <.030 <.050 <.060 <.025 <.050
NY07 08-08-00 1410 do. <.080 <.350 .19 <.500 <.200 .04 <.050 <.060 <.025 <.050
NY07 08-08-00 1415 duplicate <.080 <.350 .16 <.500 <.200 .03 <.050 <.060 <.025 <.050
NY08 08-30-00 1430 regular <.080 <.250 .07 <.500 .68 E.006 <.050 <.060 E.02 <.060
NY09 08-10-00 1215 do. <.080 <.350 <.080 <.500 <.200 .06 <.050 <.060 <.025 <.050
NY10 08-10-00 1120 do. <.080 <.350 .82 E.2 5.8 <.030 <.050 <.060 E.02 <.050
NY11 08-10-00 1609 blank <.080 <.350 <.080 <.500 <.200 <.030 <.050 <.060 <.025 <.050
NY11 08-10-00 1625 regular <.080 <.350 <.080 <.500 <.200 <.030 <.050 <.060 <.025 <.050
NY12 08-10-00 1515 do. <.080 <.350 <.080 E.2 <.200 <.030 <.050 <.060 <.025 <.050
OH01 10-05-00 1110 do. <.080 <.350 <.080 E.2 .25 1.2 <.050 <.060 .08 .53
OH02 05-24-99 1015 do. <.080 -- -- E.2 .60 .21 <.050 <.060 <.030 E.06
OH03 05-06-99 1045 do. -- -- -- -- -- -- -- -- -- --
OH04 05-06-99 1340 do. -- -- -- -- -- -- -- -- -- --
OH05 07-13-00 1130 do. <.080 <.250 .05 <.500 .21 .04 <.050 <.060 <.020 <.050
OH06 05-24-99 1245 do. -- -- -- -- -- -- -- -- -- --
OH07 06-02-99 1145 do. -- -- -- -- -- -- -- -- -- --
OH08 06-14-99 1120 do. <.080 -- -- <.500 .14 .02 <.050 <.060 <.030 <.060
OK01 05-13-99 1315 do. <.080 -- -- <.500 .54 <.030 <.050 <.060 <.030 <.060
OK03 05-03-99 1045 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
OK04 05-24-99 1300 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
OR02 07-10-00 1400 do. <.080 <.250 <.040 <.500 <.070 <.030 <.050 <.060 <.030 <.060
OR03 06-03-00 1030 do. <.080 <.250 .04 <.500 .27 <.030 <.050 <.060 E.02 <.060
OR04 07-24-00 1130 do. <.080 <.250 E.03 <.500 E.1 <.030 <.050 <.060 E.02 <.060
PA01 05-24-99 1030 do. -- -- -- -- -- -- -- -- -- --
PA02 06-08-99 1120 do. -- -- -- -- -- -- -- -- -- --
PA03 05-27-99 1520 do. -- -- -- -- -- -- -- -- -- --
PA04 05-27-99 1000 do. <.080 -- -- <.500 .20 E.02 <.050 <.060 .05 E.02
PA05 05-27-99 1150 do. -- -- -- -- -- -- -- -- -- --
TX01 08-09-99 0830 do. <.080 -- -- <.500 .75 <.030 E.02 <.060 <.030 <.060
UT01 06-14-99 1140 do. <.080 -- -- <.500 <.070 E.02 <.050 <.060 <.030 <.060
VA01 08-01-00 1500 do. <.080 <.250 E.02 <.500 <.200 <.030 <.050 <.060 <.020 <.050
WA01 07-19-00 0930 do. <.080 <.250 E.02 <.500 <.200 <.030 <.050 <.060 E.02 <.060
WA02 05-18-99 1530 do. -- -- -- -- -- -- -- -- -- --
WA03 05-14-99 1530 do. E.01 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
WA04 05-06-99 1050 do. -- -- -- -- -- -- -- -- -- --
WA05 05-14-99 1200 do. -- -- -- -- -- -- -- -- -- --
WA06 03-29-00 1000 do. <.080 <.250 E.03 <.500 <.070 <.030 <.050 <.060 <.030 <.060
WI01 04-23-99 0955 do. -- -- -- -- -- -- -- -- -- --
WI02 04-23-99 0910 do. <.080 -- -- <.500 <.070 <.030 <.050 <.060 <.030 <.060
WI03 05-17-99 1230 do. -- -- -- -- -- -- -- -- -- --
WI04 04-23-99 1450 do. -- -- -- -- -- -- -- -- -- --
WI05 04-23-99 1115 do. -- -- -- -- -- -- -- -- -- --
WI06 04-23-99 1330 do. -- -- -- -- -- -- -- -- -- --
WI07 04-23-99 0820 do. -- -- -- -- -- -- -- -- -- --

Table 5. Selected compounds, Method 4 - Continued


 
Site code Date (month-day-year) Time (24-hour) Type of sample Phenol (108-95-2) Phthalic anhydride (85-44-9) Pyrene (129-00-0) Stigmastanol (19466-47-8) Tetra-chloroethylene (127-18-4) Triclosan (3380-34-5) Tri (2-chloro-ethyl) phosphate (115-96-8) Tri (di-chloriso-propyl) phosphate (13674-87-8) Triphenyl phosphate (115-86-6)
AR02 05-02-99 1630 regular -- -- -- -- -- -- -- -- --
AR06 05-04-99 2050 do. <0.080 <0.150 0.19 -- <0.030 <0.040 <.040 <0.100 E0.01
AZ01 06-29-00 1115 do. <.250 E.7 .11 <2.000 <.030 .23 .17 <.100 <.100
AZ02 06-27-00 1625 do. E.7 E1 <.030 <2.000 E.06 .32 .25 <.100 E.05
AZ03 06-29-00 0710 do. <.080 E.6 <.030 <2.000 <.030 .73 .43 <.100 .17
AZ04 06-27-00 1035 do. <.080 <.150 <.030 <2.000 <.030 .20 .20 <.100 E.02
CA01 05-18-00 1130 do. <.080 <.150 <.030 <2.000 <.030 <.040 <.040 <.100 <.100
CA02 06-28-00 1300 do. <.080 <.150 <.030 <2.000 <.030 .06 E.02 <.100 E.002
CA03 08-16-00 1700 do. <.080 E.7 <.030 <2.000 <.030 .41 .53 <.100 E.08
CA04 08-09-00 1700 do. E.4 <.150 <.030 <2.000 E.02 .08 .30 <.100 <.100
CA05 04-15-99 1700 do. -- -- -- -- -- -- -- -- --
CA06 04-11-99 0715 do. <.080 <.200 <.030 -- <.030 .10 <.040 <.100 <.100
CA07 09-21-99 1110 do. <.150 <.200 <.030 -- <.030 .04 .05 <.100 <.100
CA08 09-21-99 1600 do. <.150 <.200 <.030 -- <.030 <.040 <.040 <.100 <.100
CA09 09-22-99 1120 do. <.150 <.200 <.030 -- <.030 E.01 <.040 <.100 <.100
CA10 09-22-99 1320 do. <.150 <.200 <.030 -- <.030 <.040 <.040 <.100 <.100
CO01 04-21-99 1250 do. <.080 E1 <.030 -- E.2 2.3 .54 <.100 <.100
DE01 05-23-99 1130 do. <.080 <.150 <.030 -- <.030 .04 <.040 <.100 <.100
DE01 05-23-99 1140 duplicate <.080 <.150 <.030 -- <.030 .04 <.040 <.100 <.100
FL01 08-28-00 1215 regular <.45 <.35 <.030 <2.000 <.030 <.050 .13 <.100 <.100
FL02 08-23-00 1215 do. <.45 <.35 <.030 <2.000 <.030 E.04 .05 <.100 <.100
GA01 05-26-99 1400 do. -- -- -- -- -- -- -- -- --
GA02 05-25-99 1130 do. -- -- -- -- -- -- -- -- --
GA03 05-25-99 1030 do. -- -- -- -- -- -- -- -- --
GA04 05-25-99 0840 do. <.080 E1 <.030 -- <.030 .27 <.040 <.100 <.100
GA05 05-26-99 1130 do. -- -- -- -- -- -- -- -- --
GA06 05-24-99 1215 do. -- -- -- -- -- -- -- -- --
GA07 05-31-00 1115 do. <.080 <.150 .04 <2.000 <.030 .26 E.09 <.100 E.03
IA01 09-13-00 1600 do. <.250 E.7 <.030 <2.000 <.030 <.040 <.040 <.100 <.100
IA02 09-12-00 1200 do. <.250 <.290 <.030 <2.000 <.030 <.040 .04 <.100 <.100
IA04 09-11-00 1700 do. <.250 <.250 <.030 <2.000 E.02 .14 <.040 .14 <.100
IA05 04-05-99 1445 do. -- -- -- -- -- -- -- -- --
IA07 04-08-99 1000 do. -- -- -- -- -- -- -- -- --
IA08 04-06-99 0935 do. -- -- -- -- -- -- -- -- --
IA09 04-06-99 1245 do. <.080 E.6 <.030 -- <.030 .04 .06 <.100 <.100
IA10 04-04-99 2000 do. -- -- -- -- -- -- -- -- --
IA11 04-03-99 1855 do. -- -- -- -- -- -- -- -- --
IA12 04-03-99 1245 do. -- -- -- -- -- -- -- -- --
ID01 08-14-00 1110 do. -- -- -- -- -- -- -- -- --
ID02 08-15-00 1250 do. <.450 <.350 <.030 <2.000 <.030 E.04 <.040 <.100 <.100
ID03 08-16-00 1222 do. E.3 <.350 <.030 <2.000 <.030 .04 <.040 <.100 <.100
ID04 05-17-00 1215 do. <.080 <.150 <.030 <2.000 <.030 <.040 <.040 <.100 <.100
IL01 05-13-99 1300 do. -- -- -- -- -- -- -- -- --
IL02 05-17-99 1420 do. -- -- -- -- -- -- -- -- --
IL03 09-06-00 1050 do. <.250 E.6 E.05 <2.000 <.030 .10 .22 .10 <.100
IL04 09-06-00 0940 do. <.250 <.250 E.1 <2.000 <.030 .11 .19 .11 <.100
IL05 05-20-99 0810 do. <.080 E.9 .27 -- E.2 .30 .27 <.100 <.100
IL06 05-17-99 1230 do. -- -- -- -- -- -- -- -- --
IL07 05-13-99 1710 do. -- -- -- -- -- -- -- -- --
LA01 04-19-99 1130 do. <.080 <.150 <.030 -- <.030 <.040 <.040 <.100 <.100
MA01 05-12-99 0840 do. -- -- -- -- -- -- -- -- --
MA02 07-25-00 0630 do. E.5 <.250 <.030 <2.000 E.1 .09 .05 E.09 <.100
MA03 07-25-00 0750 blank <.250 <.250 <.030 <2.000 <.030 <.040 <.040 .08 <.100
MA03 07-25-00 0800 regular <.250 <.250 <.030 <2.000 E.07 .12 E.04 .11 <.100
MA03 07-25-00 0810 duplicate <.250 <.250 <.030 <2.000 <.030 .07 .05 E.08 <.100
MA04 07-25-00 0900 regular <.250 <.250 <.030 <2.000 E.7 .16 .07 .16 <.100
MA05 07-25-00 1100 do. E.2 <.250 <.030 <2.000 <.030 .08 .05 .08 <.100
MA06 07-25-00 1010 do. <.250 <.250 <.030 <2.000 E.5 .15 .04 .15 <.100
MA07 07-25-00 1130 do. <.250 <.250 E.05 <2.000 E.07 <.040 <.040 <.100 <.100
MD01 09-17-99 0930 do. -- -- -- -- -- -- -- -- --
MD02 05-19-99 1710 do. -- -- -- -- -- -- -- -- --
MI01 06-15-99 1030 do. -- -- -- -- -- -- -- -- --
MI02 06-15-99 1430 do. -- -- -- -- -- -- -- -- --
MI03 06-16-99 1045 do. <.080 <.150 <.030 -- <.030 <.040 .18 <.100 <.100
MN03 10-03-00 1105 blank E3 <.350 <.030 <2.000 <.030 <.050 <.040 <.100 <.100
MN03 10-03-00 1115 regular E.4 <.350 <.030 <2.000 <.030 .05 <.040 <.100 <.100
MN04 10-02-00 1210 do. E.6 E.7 .03 <2.000 <.030 .11 .10 <.100 <.100
MO01 05-06-99 1130 do. <.080 <.150 .05 -- <.030 .46 .08 <.100 <.100
MO02 04-29-99 1245 do. <.080 <.150 <.030 -- E.07 1.0 .15 <.100 <.100
MO03 04-30-99 0830 do. <.080 <.150 <.030 -- E.04 .46 .07 <.100 <.100
MO04 04-30-99 1300 do. <.080 <.150 .06 -- E.05 .67 .11 <.100 <.100
MO05 05-15-99 1315 do. <.080 <.150 E.02 -- <.030 <.040 <.040 <.100 <.100
MO06 04-07-99 0845 do. <.080 <.150 <.030 -- <.030 <.040 <.040 <.100 <.100
MO07 04-05-99 1530 do. -- -- -- -- -- -- -- -- --
MO08 04-07-99 0840 do. -- -- -- -- -- -- -- -- --
MT01 03-16-00 1040 do. .22 <.150 <.030 <2.000 E.02 .09 <.040 <.100 <.100
MT02 03-16-00 1400 do. <.080 <.150 <.030 <2.000 <.030 1.7 .08 <.100 E.08
MT03 03-17-00 1100 do. .16 <.150 <.030 <2.000 E.2 <.040 .40 <.100 E.03
MT04 03-06-00 1400 do. <.080 <.150 <.030 E4 <.030 <.040 .08 <.100 .10
MT05 03-22-00 1130 do. <.080 <.150 <.030 <2.000 <.030 <.040 <.040 <.100 <.100
NC01 05-06-99 1015 do. -- -- -- -- -- -- -- -- --
NC02 05-06-99 1230 do. -- -- -- -- -- -- -- -- --
NC03 05-06-99 1430 do. -- -- -- -- -- -- -- -- --
NC04 05-06-99 1545 do. -- -- -- -- -- -- -- -- --
NC05 05-13-99 1245 do. -- -- -- -- -- -- -- -- --
NE01 06-24-99 1330 do. -- -- -- -- -- -- -- -- --
NE02 06-15-99 1730 do. <.080 <.150 <.030 -- <.030 <.040 <.040 <.100 <.100
NE03 06-14-99 1600 do. .17 <.150 <.030 -- <.030 <.040 .10 <.100 <.100
NE04 06-15-99 1700 do. -- -- -- -- -- -- -- -- --
NE05 06-03-99 1230 do. -- -- -- -- -- -- -- -- --
NE06 06-04-99 1030 do. -- -- -- -- -- -- -- -- --
NE07 06-17-99 1130 do. -- -- -- -- -- -- -- -- --
NJ01 06-01-99 1020 do. -- -- -- -- -- -- -- -- --
NJ02 08-15-00 1300 do. E.2 <.290 .19 <2.000 <.030 <.050 .06 <.100 <.100
NJ03 08-17-00 1040 do. E.8 <.150 <.030 <2.000 <.030 E.03 .04 <.100 <.100
NJ04 05-27-99 1120 do. -- -- -- -- -- -- -- -- --
NY01 03-28-00 1310 do. .40 <.150 .10 E.6 <.030 .25 .19 <.100 .22
NY02 08-08-00 1150 do. E.3 <.350 .07 <2.000 <.030 <.050 <.040 <.100 <.100
NY03 08-23-00 1340 do. E.3 <.350 .05 <2.000 <.030 .44 .05 <.100 <.100
NY04 08-08-00 1100 do. E.2 <.350 <.030 <2.000 <.030 <.050 <.040 <.100 <.100
NY05 08-08-00 1300 do. E.4 <.350 .06 <2.000 E.1 <.050 <.040 <.100 <.100
NY06 08-08-00 1500 do. E.3 <.350 <.030 <2.000 E.04 <.050 <.040 <.100 <.100
NY07 08-08-00 1410 do. E.3 <.350 .03 <2.000 <.030 .09 .15 <.100 <.100
NY07 08-08-00 1415 duplicate E.3 <.350 <.030 <2.000 <.030 .06 .12 <.100 <.100
NY08 08-30-00 1430 regular E1 <.250 E.006 <2.000 <.030 <.040 .10 <.100 <.100
NY09 08-10-00 1215 do. E.3 <.350 .05 <2.000 <.030 <.050 <.040 <.100 <.100
NY10 08-10-00 1120 do. E.3 E1 <.030 <2.000 <.030 .50 .11 <.100 <.100
NY11 08-10-00 1609 blank E.3 <.350 <.030 <2.000 <.030 <.050 <.040 <.100 <.100
NY11 08-10-00 1625 regular E.3 <.350 <.030 <2.000 <.030 <.050 <.040 <.100 <.100
NY12 08-10-00 1515 do. E.3 <.350 <.030 <2.000 E.1 <.050 <.040 <.100 <.100
OH01 10-05-00 1110 do. <.450 <.350 .84 E2 <.030 .62 E.04 <.100 <.100
OH02 05-24-99 1015 do. <.080 E.8 .15 -- E.08 .14 .10 <.100 <.100
OH03 05-06-99 1045 do. -- -- -- -- -- -- -- -- --
OH04 05-06-99 1340 do. -- -- -- -- -- -- -- -- --
OH05 07-13-00 1130 do. E1 E.3 E.03 <2.000 <.030 <.040 .04 <.100 <.100
OH06 05-24-99 1245 do. -- -- -- -- -- -- -- -- --
OH07 06-02-99 1145 do. -- -- -- -- -- -- -- -- --
OH08 06-14-99 1120 do. <.080 <.150 E.02 -- <.030 <.040 .13 <.100 <.100
OK01 05-13-99 1315 do. <.080 E.2 <.030 -- <.030 .17 <.040 <.100 <.100
OK03 05-03-99 1045 do. <.080 <.150 <.030 -- <.030 <.040 <.040 <.100 <.100
OK04 05-24-99 1300 do. <.080 <.150 <.030 -- <.030 <.040 <.040 <.100 <.100
OR02 07-10-00 1400 do. .35 <.150 <.030 <2.000 <.030 .43 <.040 <.100 <.100
OR03 06-03-00 1030 do. <.080 <.150 <.030 <2.000 <.030 .17 .12 <.100 E.02
OR04 07-24-00 1130 do. <.25 <.250 <.030 <2.000 <.030 .09 .04 E.09 <.100
PA01 05-24-99 1030 do. -- -- -- -- -- -- -- -- --
PA02 06-08-99 1120 do. -- -- -- -- -- -- -- -- --
PA03 05-27-99 1520 do. -- -- -- -- -- -- -- -- --
PA04 05-27-99 1000 do. <.080 E.6 E.02 -- <.030 .06 .06 <.100 <.100
PA05 05-27-99 1150 do. -- -- -- -- -- -- -- -- --
TX01 08-09-99 0830 do. <.150 E.8 <.030 -- <.030 .30 .42 <.100 <.100
UT01 06-14-99 1140 do. <.080 <.150 <.030 -- E.02 <.040 .05 <.100 <.100
VA01 08-01-00 1500 do. E.5 <.290 <.030 <2.000 <.030 <.050 <.040 <.100 <.100
WA01 07-19-00 0930 do. <.250 <.250 <.030 <2.000 <.030 .07 E.03 E.08 <.100
WA02 05-18-99 1530 do. -- -- -- -- -- -- -- -- --
WA03 05-14-99 1530 do. <.080 <.150 <.030 -- <.030 <.040 <.040 <.100 <.100
WA04 05-06-99 1050 do. -- -- -- -- -- -- -- -- --
WA05 05-14-99 1200 do. -- -- -- -- -- -- -- -- --
WA06 03-29-00 1000 do. .08 <.150 <.030 <2.000 <.030 <.040 <.040 <.100 <.100
WI01 04-23-99 0955 do. -- -- -- -- -- -- -- -- --
WI02 04-23-99 0910 do. <.080 <.150 <.030 -- <.030 <.040 <.040 <.100 <.100
WI03 05-17-99 1230 do. -- -- -- -- -- -- -- -- --
WI04 04-23-99 1450 do. -- -- -- -- -- -- -- -- --
WI05 04-23-99 1115 do. -- -- -- -- -- -- -- -- --
WI06 04-23-99 1330 do. -- -- -- -- -- -- -- -- --
WI07 04-23-99 0820 do. -- -- -- -- -- -- -- -- --

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