The Chemical Analysis of Argonne Premium Coal Samples
Edited by Curtis A. Palmer
1997
U.S. Geological Survey Bulletin 2144
Compilation of Multitechnique Determinations of 51 Elements in 8 Argonne Premium Coal Samples
By Curtis A. Palmer and Sarah A. Klizas
Table 4. Agreement between techniques for trace elements using data from table 2 and criteria described in the text -- continued.
| Element | HP techniques |
Overall agreement |
Exceptions | LP techniques |
Overall agreement |
Exceptions |
| Sr | INAA(A) | Good | 1,3,6u | EDXRF(C) | Good | 2,5,7,8u |
| EDXRF(A) | Good | 7,8u;6x | DCAES(A) | Usable | 1,5g;4,6p | |
| ICAP-AES(A) | Usable | 1,4,6g;2fp | ||||
| ICAP-AES(A)* | Good | 8u | ||||
| Y | EDXRF(A) | Usable | 1-3,5g;6,8x;7fp | EDXRF(C) | Usable | (6)sg,7p;1-5, 8x |
| ICAP-AES(A) | Good | 8u | DCAES(A) | Usable | 1p | |
| ICAP-AES(A)* | Good | 1u | ||||
| Zr | ICAP-AES(A)* | Good | 8u,6= | EDXRF(C) | Usable | 2,3,6g;8p |
| EDXRF(A) | Good | 8u;6x | DCAES(A) | Usable | 1,7,8p | |
| DCAES(C) | Usable | 3g;5p;2,6-8x | ||||
| Nb | ICAP-MS(A)* | Good | 2,7u;6,8= | EDXRF(C) | Poor | 1-6,8x |
| EDXRF(A) | Usable | 1,3,4g;6,8x | DCAES(A) | Usable | 4,6g;7p | |
| Mo | ICAP-MS(A)* | -- | 1-8= | DCAES(A) | Usable | 4g;1,8p |
| Ag | ICAP-MS(A)* | -- | 1-8= | DCAES(A) | Poor | 8x |
| Cd | ICAP-MS(A)* | Usable | 5,6,8g;1p | |||
| GFAAS(A) | Usable | 5,8g | ||||
| Sn | ICAP-MS(A)* | -- | 1-8= | DCAES(A) | Poor | 7g |
| Sb | INAA(C) | Good | 5u | |||
| ICAP-MS(A)* | Good | 5u | ||||
| Cs | INAA(C) | Good | 1,3,7u | |||
| ICAP-MS(A)* | Good | 1,3,7u | ||||
| Ba | INAA(C) | Good | 3,4,8u | EDXRF(C) | Usable | 1g;2,3,7,8p |
| EDXRF(A) | Good | 4,7,8u;6x | DCAES(A) | Good | 1,3,8u | |
| ICAP-AES(A) | Usable | 1,3,4,6,7g;2f,5fp | DCAES(C) | Poor | 2u;6-8x | |
| ICAP-AES(A)* | Good | |||||
| La | INAA(C) | Usable | 3,5g | EDXRF(C) | Poor | 2s,5s,7u;4s,6s,8s |
| ICAP-MS(A)* | Usable | 5,3,7g | ||||
| EDXRF(A) | Usable | 1,7g;5fp;2,3,6,8x | DCAES(A) | Usable | 6g;3,8p | |
| Ce | INAA(C) | Good | 2-5u | EDXRF(C) | Poor | 5g |
| ICAP-MS(A)* | Good | 3,5u | DCAES(A) | Poor | 2,5,7u;4,8x | |
| EDXRF(A) | Usable | 1g;6,8x | ||||
| Pr | ICAP-MS(A)* | -- | 1-8= | DCAES(A) | Poor | 6u;1-5,8x |
| Nd | INAA(C) | Usable | (1),6g;2-5x | DCAES(A) | Usable | 1s,4g;7p;2,8x |
| ICAP-MS(A)* | Good | 8u;2-5= | ||||
| Sm | INAA(C) | Usable | 3g | DCAES(A) | Poor | 5,6u;1-4x |
| ICAP-MS(A)* | Usable | 3g | ||||
| Eu | INAA(C) | Good | 4,8u | DCAES(A) | Usable | 6u,7g;1-5,8x |
| ICAP-MS(A)* | Good | 4,8u | ||||
| Tb | INAA(C) | Good | ||||
| ICAP-MS(A)* | Good | |||||
| Yb | INAA(C) | Good | 8u | DCAES(A) | Usable | 1,6,7g |
| ICAP-MS(A)* | Good | 8u | ||||
| Hf | INAA(C) | Good | 1,3,5,7u | |||
| ICAP-MS(A)* | Good | 1,3,5,7u |
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