Gas-liquid chromatographic determination of 3-trifluoromethyl-4-nitrophenol residues in fish
Journal of the Association of Official Analytical Chemists
By: J.L. Allen and J.B. Sills
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Abstract
A procedure for the determination of 3-trifluormethyl-4-nitrophenol (TFM) in fish tissues is described. Homogenized tissues are extracted with hexane-ethyl ether; the extract is cleaned up by partitioning the TFM from the extracting solvent into 0.1N NaOH, acidifying the aqueous solution, and partitioning again with hexaneethyl ether. The TFM is methylated with diazomethane and analyzed by gas-liquid chromatography, using electron capture detection. Recoveries ranged from 75 to 100% from fish muscles that were spiked with 0.01—2.00 μg TFM/g.
| Publication type | Article |
|---|---|
| Publication Subtype | Journal Article |
| Title | Gas-liquid chromatographic determination of 3-trifluoromethyl-4-nitrophenol residues in fish |
| Series title | Journal of the Association of Official Analytical Chemists |
| DOI | 10.1093/jaoac/57.2.387 |
| Volume | 57 |
| Issue | 2 |
| Publication Date | February 13, 2020 |
| Year Published | 1974 |
| Language | English |
| Publisher | Oxford Academic |
| Contributing office(s) | Upper Midwest Environmental Sciences Center |
| Description | 2 p. |
| First page | 387 |
| Last page | 388 |
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