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Abstract
A method is described for the analysis of polychlorinated biphenyl (PCB) compounds in tissue samples. Cleanup by hexane-aceto-nitrile partitioning and Florisil column chromatography are performed on samples before oxidative treatment to convert DDE to DCBP. PCB components are then determined semi-quantitatively by TLC. No prior separation of PCB from chlorinated pesticides is required. The lower limit of sensitivity is 0.2 ?g.
| Publication type | Article |
|---|---|
| Publication Subtype | Journal Article |
| Title | Evidence of decline for Bufo boreas and Rana luteiventris in and around the northern Great Basin |
| Series title | Alytes |
| Volume | 22 |
| Issue | 3-4 |
| Year Published | 2005 |
| Language | English |
| Contributing office(s) | Forest and Rangeland Ecosystem Science Center |
| Description | p. 95-108 |
| Larger Work Type | Article |
| Larger Work Subtype | Journal Article |
| Larger Work Title | Alytes |
| First page | 95 |
| Last page | 108 |
| Google Analytic Metrics | Metrics page |