Determination of rhenium in molybdenite by X-ray fluorescence. A combined chemical-spectrometric technique
Talanta
By: M.W. Solt, J.S. Wahlberg, and A.T. Myers
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Abstract
Rhenium in molybdenite is separated from molybdenum by distillation of rhenium heptoxide from a perchloric-sulphuric acid mixture. It is concentrated by precipitation of the sulphide and then determined by X-ray fluorescence. From 3 to 1000 μg of rhenium can be measured with a precision generally within 2%. The procedure tolerates larger amounts of molybdenum than the usual colorimetric methods.
Suggested Citation
Solt, M., Wahlberg, J., Myers, A., 1969, Determination of rhenium in molybdenite by X-ray fluorescence. A combined chemical-spectrometric technique: Talanta, v. 16, no. 1, p. 37-43, https://doi.org/10.1016/0039-9140(69)80238-9.
| Publication type | Article |
|---|---|
| Publication Subtype | Journal Article |
| Title | Determination of rhenium in molybdenite by X-ray fluorescence. A combined chemical-spectrometric technique |
| Series title | Talanta |
| DOI | 10.1016/0039-9140(69)80238-9 |
| Volume | 16 |
| Issue | 1 |
| Year Published | 1969 |
| Language | English |
| Publisher | Elsevier |
| Description | 7 p. |
| First page | 37 |
| Last page | 43 |