Nuclear magnetic resonance studies of the phosphorus(v) pesticides: A rapid determination of the isomer ratio of systox
Analytica Chimica Acta
By: H. Babad, T.N. Taylor, and M. C. Goldberg
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Abstract
The integration circuit of the Varian A-60 nuclear magnetic resonance spectrometer is used in conjunction with vapor phase chromatography, to develop a rapid analysis technique for the determination of isomer ratios in technical Systox-Sulfotepp mixtures. The complete analysis requires less than 0.1 g of sample and only 15 min. The isomer ratio in the sample may be determined to an accuracy of ±1.5% and the undamaged sample may be recovered.
Suggested Citation
Babad, H., Taylor, T., and Goldberg, M.C., 1968, Nuclear magnetic resonance studies of the phosphorus(v) pesticides: A rapid determination of the isomer ratio of systox: Analytica Chimica Acta, v. 40, no. C, p. 387-392, https://doi.org/10.1016/S0003-2670(00)86752-5.
| Publication type | Article |
|---|---|
| Publication Subtype | Journal Article |
| Title | Nuclear magnetic resonance studies of the phosphorus(v) pesticides: A rapid determination of the isomer ratio of systox |
| Series title | Analytica Chimica Acta |
| DOI | 10.1016/S0003-2670(00)86752-5 |
| Volume | 40 |
| Issue | C |
| Year Published | 1968 |
| Language | English |
| Publisher | Elsevier |
| Description | 6 p. |
| First page | 387 |
| Last page | 392 |