Spectrophotometric determination of fluorine in silicate rocks

Talanta
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Abstract

The rock powder is sintered with a sodium carbonate flux containing zinc oxide and magnesium carbonate, the sinter-cake leached with water and the resulting solution filtered. Fluorine is separated from the acidified filtrate by steam distillation and determined spectrophotometrically by means of a zirconium-SPADNS reagent. If a multiple-unit distillation apparatus is used, 12 determinations can be completed per man-day.

Publication type Article
Publication Subtype Journal Article
Title Spectrophotometric determination of fluorine in silicate rocks
Series title Talanta
DOI 10.1016/0039-9140(64)80192-2
Volume 11
Issue 9
Year Published 1964
Language English
Publisher Elsevier
Description 5 p.
First page 1343
Last page 1347
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