Spectrophotometric determination of fluorine in silicate rocks
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Abstract
The rock powder is sintered with a sodium carbonate flux containing zinc oxide and magnesium carbonate, the sinter-cake leached with water and the resulting solution filtered. Fluorine is separated from the acidified filtrate by steam distillation and determined spectrophotometrically by means of a zirconium-SPADNS reagent. If a multiple-unit distillation apparatus is used, 12 determinations can be completed per man-day.
Publication type | Article |
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Publication Subtype | Journal Article |
Title | Spectrophotometric determination of fluorine in silicate rocks |
Series title | Talanta |
DOI | 10.1016/0039-9140(64)80192-2 |
Volume | 11 |
Issue | 9 |
Year Published | 1964 |
Language | English |
Publisher | Elsevier |
Description | 5 p. |
First page | 1343 |
Last page | 1347 |
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