Routine low-level monitoring of polar pesticides and pesticide degradates by HPLC/ESI-MS: Evaluating long-term performance
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Abstract
The sensitivity and selective determination of polar pesticides were analyzed using high-performance liquid chromatography/electrospray ionization-mass spectrometry (HPLC/ESI-MS). The effects of multiple operators and instruments on method performance were evaluated using 440 pairs of fortified reagent-water and blank reagent-water samples. The influence of varying environmental matrices on recovery and precision were also analyzed using 200 fortified ambient water samples and duplicate ambient water samples. The results show that compound stability in filtered water was matrix-, chemical class- and compound-dependent which ranged from 1 day to 2 weeks.
Suggested Citation
Furlong, E., Martin, J., Werner, S., Gates, P.M., 2002, Routine low-level monitoring of polar pesticides and pesticide degradates by HPLC/ESI-MS: Evaluating long-term performance, in Proceedings 50th ASMS Conference on Mass Spectrmetry and Allied Topics, Orlando, FL, 2 June 2002 through 6 June 2002, p. 651-652.
| Publication type | Conference Paper |
|---|---|
| Publication Subtype | Conference Paper |
| Title | Routine low-level monitoring of polar pesticides and pesticide degradates by HPLC/ESI-MS: Evaluating long-term performance |
| Year Published | 2002 |
| Language | English |
| Larger Work Title | Proceedings 50th ASMS Conference on Mass Spectrmetry and Allied Topics |
| First page | 651 |
| Last page | 652 |
| Conference Title | Porceedings - 50th ASMS Conference on Mass Spectrometry and Allied Topics |
| Conference Location | Orlando, FL |
| Conference Date | 2 June 2002 through 6 June 2002 |