Applying the silver-tube introduction method for thermal conversion elemental analyses and a new δ2H value for NBS 22 oil
Rapid Communications in Mass Spectrometry
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Abstract
The δ2HVSMOW–SLAP value of total hydrogen of the international measurement standard NBS 22 oil was determined by a new method of sealing water in silver tubes for use in a thermal conversion elemental analysis (TC/EA) reduction unit. The isotopic fractionation of water due to evaporation is virtually non-existent in this silver-tube method. A new value for the δ2HVSMOW–SLAP of NBS 22 oil, calibrated with isotopic reference waters, was determined to be −116.9 ± 0.8‰ (1σ and n = 31).
| Publication type | Article |
|---|---|
| Publication Subtype | Journal Article |
| Title | Applying the silver-tube introduction method for thermal conversion elemental analyses and a new δ2H value for NBS 22 oil |
| Series title | Rapid Communications in Mass Spectrometry |
| DOI | 10.1002/rcm.4638 |
| Volume | 24 |
| Issue | 15 |
| Publication Date | July 13, 2010 |
| Year Published | 2010 |
| Language | English |
| Publisher | Wiley |
| Publisher location | Hoboken, NJ |
| Description | 8 p. |
| Larger Work Type | Article |
| Larger Work Subtype | Journal Article |
| Larger Work Title | Rapid Communications in Mass Spectrometry |
| First page | 2269 |
| Last page | 2276 |