X-ray fluorescence determination of sodium in silicate standards using direct dilution and dilution fusion preparation techniques
X-ray Spectrometry
By: B.P. Fabbi
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Abstract
Direct dilution of a sample with an equal proportion of cellulose binder and dilution fusion of one part of sample with fourteen parts of LiBO2 flux has been used to prepare pelletized samples of silicate standards for determining sodium by X-ray fluorescence analysis. An RAP analysing crystal was used to disperse and reflect the sodium spectra. Detection limits were found to be 0.07 and 0.39% Na2O at the 2s̀ confidence level for the direct dilution and dilution fusion preparation techniques, respectively.
| Publication type | Article |
|---|---|
| Publication Subtype | Journal Article |
| Title | X-ray fluorescence determination of sodium in silicate standards using direct dilution and dilution fusion preparation techniques |
| Series title | X-ray Spectrometry |
| DOI | 10.1002/xrs.1300020106 |
| Volume | 2 |
| Issue | 1 |
| Year Published | 1973 |
| Language | English |
| Publisher | Wiley |
| Description | 3 p. |
| First page | 15 |
| Last page | 17 |
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