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COMMON
CHN PROBLEMS
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Listed below in tabular and prose format are some common problems associated with running the CHN Analyzer. As difficulties are encountered, one may also refer to the Perkin Elmer manual. Error messages and their associated numbers are listed there in the 'Messages' section. Some examples: |
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After changing the tubes,
run Leak Tests. Message 10 means the Hydrogen K-Factor is out of tolerance and can most likely be ignored since we do not use the Hydrogen value - press Start and the run sequence will continue. |
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If, for any reason, you must
stop the run sequence, press Single Run and the machine will finish analyzing
the present sample and then go into STANDBY. Sometimes the analyzer will not drop a sample or it will analyze two samples at once. If this happens, push SINGLE RUN to stop the machine and remove the sample from the drop hole. |
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K-factor Problems: If you need to calibrate the machine by running multiple K-factors using the Single Run mode, you can unscrew the autosampler and remove it from the machine in order to manually move the wheel back the number of spaces you require. You can analyze a couple of Single Runs of K-factors to recalibrate the machine until the values are within the limits. K-factor limits are listed in the table in the CHN Standards section. If, after analyzing a K-factor in your Auto Run, the values are more than +/- 10% of the limit listed, you'll need to stop the run and analyze K-factors until the levels are within the limit. Once the K-factor values are within the limit, move the wheel back to the next run number in your sequence, use the micro forceps to add the next sample to the drop hole, and press START to resume the Auto Run. |
Common Problems:
Error Message
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Associated Message Printed
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Recommended Action
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4, 5
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Change Reduction/Combustion Tube | Change tube and reset Run Counter |
6
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Empty Vial Receptacle | Empty Receptacle and reset Run Counter |
8
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Check for Sample Drop | Adjust Autosampler alignment with drop hole |
10, 11, 12
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C, H, N K-factor out of tolerance | Run more K-factors until values are within the limit posted |
15, 16, 17
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C, H, N Blank out of tolerance | Run more blanks until values are within the limit posted |
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