The U.S. Geological Survey initiated an urban water-quality study in 1979 in cooperation with the City of Charlotte and Mecklenburg County, North Carolina. As part of this study, a water-quality monitoring network was established at selected landfill sites in Mecklenburg County. Water-quality samples were collected at 27 surface-water sites and 97 ground-water sites at 5 landfills from 1979-92. Samples were analyzed for selected physical and biological characteristics, major inorganic ions, nutrients, trace elements, organic compounds, and suspended sediment. Analyses for constituents of concern are presented in tables and as graphical time series plots. Results from all analyses are compiled in tabular form in appendixes.